| 高速逆流制备分离中药黄柏中的生物碱 |
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| 引用本文： | 袁黎明,吴平,夏滔,谌学先.高速逆流制备分离中药黄柏中的生物碱[J].色谱,2002,20(2):185-186. |
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| 作者姓名： | 袁黎明 吴平 夏滔 谌学先 |
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| 作者单位： | 1. 云南师范大学化学化工学院,云南,昆明,650092
2. 云南师范大学科研处,云南,昆明,650092 |
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| 基金项目： | 云南省自然科学基金资助课题 ( 2 0 0 0B0 0 45M ) |
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| 摘 要： | 利用高速逆流对传统中药黄柏中的生物碱类活性成分进行了制备分离。两相溶剂分离系统采用氯仿 甲醇 0 5mol/LHCl(体积比为 2∶1∶1) ,并对制备物进行了薄层分析。证实了生物碱成分 ,检出了小檗碱。
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| 关 键 词： | 高速逆流 制备分离 生物碱 黄柏 |
| 文章编号： | 1000-8713(2002)02-0185-02 |
| 修稿时间： | 2001年9月27日 |
Preparative Separation of Alkaloids from Cortex Phellodendri by High Speed Countercurrent Chromatography |
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| YUAN Li-ming ,WU Ping ,XIA Tao ,CHEN Xue-xian.Preparative Separation of Alkaloids from Cortex Phellodendri by High Speed Countercurrent Chromatography[J].Chinese Journal of Chromatography,2002,20(2):185-186. |
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| Authors: | YUAN Li-ming WU Ping XIA Tao CHEN Xue-xian |
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| Institution: | College of Chemistry and Chemical Engineering, Yunnan Normal University, Kunming 650092, China. yuanlm@public.km.yn.cn |
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| Abstract: | High speed countercurrent chromatography was successfully applied to the separation of alkaloids from Cortex Phellodendri with a two-phase solvent system composed of CHCl3-CH3OH-0.5 mol/L HCl (2:1:1, volume ratio). Some alkaloid components were obtained, and identification of berberine was made by thin-layer chromatography. |
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| Keywords: | high speed countercurrent chromatography preparative separation alkaloid Cortex Phellodendri |
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