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气相色谱法快速测定空气中低分子量醛
引用本文:任清,郭友嘉.气相色谱法快速测定空气中低分子量醛[J].色谱,1997,15(4):356-357.
作者姓名:任清  郭友嘉
作者单位:中国科学院福建物质结构研究所
摘    要:用填充气相色谱直接进样法测定了污染空气中甲醛、乙醛、丙醛的含量,并对方法的灵敏度、准确度及各种影响因素进行了探讨。方法用于样品测定取得了较为满意的结果。

关 键 词:丙醛  甲醛  气相色谱法  乙醛  

Rapid Determination of Low Molecular Weight Aldehydes in Air by Gas Chromatography
Ren Qing and Guo Youjia.Rapid Determination of Low Molecular Weight Aldehydes in Air by Gas Chromatography[J].Chinese Journal of Chromatography,1997,15(4):356-357.
Authors:Ren Qing and Guo Youjia
Institution:Fujian Institute of Structure of Matter, the Chinese Academy of Sciences, Fuzhou, 350002.
Abstract:This paper reports a method for determination of low molecular weight aldehydes in polluted air by GC-FID using a GDX-401 packed column (3 mm x 3 m). The advantages of this method are simple, rapid, accurate and sensitive. The method requires only 8 minutes for the whole analysis. In the concentration range of 1.7-442.4 mg/m3 for formaldehyde and 0.5-680 mg/m3 for acetaldehyde and propionaldehyde the calibration curves are linear. The minimun detectable amounts are 3.5 ng, 1 ng and 1 ng, and the average recoveries (n=5) are 89.4%, 89.6%, 88.1% for formaldehyde, acetaldehyde and propionaldehyde respectively. The quantitative determination is performed by external standard calibration method. The results of sample analysis are satisfactory.
Keywords:gas chromatography  formaldehyde  acetaldehyde  propionaldehyde
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