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Electrochemical Synthesis of Trifluoromethane Sulfinic Acid Salt From CF3Br and SO2
Authors:Jean-Claude Folest  Jean-Yves Nédélec  Jacques Périchon
Institution:Laboratoire d'Electrochimie , Catalyse et Synthèse Organique, U.M. 28, C.N.R.S., 2, rue Henri-Dunant, 94320, Thiais, France
Abstract:The electroreduction of a mixture of SO2 and CF3Br in DMF, in an undivided cell with a soluble anode (Mg or Zn) lead to salt of trifluoromethane sulfinic acid in high yield.
Keywords:
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