Electrochemical Synthesis of Trifluoromethane Sulfinic Acid Salt From CF3Br and SO2 |
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Authors: | Jean-Claude Folest Jean-Yves Nédélec Jacques Périchon |
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Institution: | Laboratoire d'Electrochimie , Catalyse et Synthèse Organique, U.M. 28, C.N.R.S., 2, rue Henri-Dunant, 94320, Thiais, France |
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Abstract: | The electroreduction of a mixture of SO2 and CF3Br in DMF, in an undivided cell with a soluble anode (Mg or Zn) lead to salt of trifluoromethane sulfinic acid in high yield. |
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