| 气相色谱-质谱法测定荷兰豆中氟硅唑、丙环唑、苯醚甲环唑残留量 |
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| 引用本文： | 王连珠,王登飞,郑俊超,王瑞龙,刘溢娜,梁鸣,卢声宇.气相色谱-质谱法测定荷兰豆中氟硅唑、丙环唑、苯醚甲环唑残留量[J].理化检验(化学分册),2006,42(12):1025-1028,1031. |
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| 作者姓名： | 王连珠 王登飞 郑俊超 王瑞龙 刘溢娜 梁鸣 卢声宇 |
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| 作者单位： | 1. 漳州出入境检验检疫局,漳州,363000
2. 福建出入境检验检疫局,福州,350001 |
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| 摘 要： | 试样经乙腈提取,Dual Layer ENVITM-CarbⅡ/PSA(500/500 mg)固相萃取柱净化,选择离子监测/全扫描(SIM/SCAN),同时采集气相色谱-质谱法(GC-MS)对荷兰豆中氟硅唑、丙环唑、苯醚甲环唑残留量进行定性定量分析,方法检出限分别为0.001,0.003,0.005 mg.kg-1,在0.01,0.02,0.05 mg.kg-1添加水平回收率分别为60%~120%,70%~112%,75%~110%,相对标准偏差为5.0%~12.0%。
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| 关 键 词： | GC-MS 固相萃取 SIM／SCAN同时采集 氟硅唑 丙环唑 苯醚甲环唑 荷兰豆 |
| 文章编号： | 1001-4020（2006）12-1025-04 |
| 收稿时间： | 2006-06-20 |
| 修稿时间： | 2006-06-20 |
GC-MS DETERMINATION OF RESIDUAL FLUOSILAZOLE PROPICONAZOLE AND DIFENOCONAZOLE IN GREEN PEA |
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| WANG Lian-zhu,WANG Deng-fei,ZHENG Jun-chao,WANG Rui-long,LIU Yi-na,LIANG Ming,LU Sheng-yu.GC-MS DETERMINATION OF RESIDUAL FLUOSILAZOLE PROPICONAZOLE AND DIFENOCONAZOLE IN GREEN PEA[J].Physical Testing and Chemical Analysis Part B:Chemical Analgsis,2006,42(12):1025-1028,1031. |
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| Authors: | WANG Lian-zhu WANG Deng-fei ZHENG Jun-chao WANG Rui-long LIU Yi-na LIANG Ming LU Sheng-yu |
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| Abstract: | |
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| Keywords: | CK -MS Solid-phase extractiom Synchronous SIM/SCAN data aquisition mode Fluosilazole Propiconazole Difenoconazole Green pea |
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