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Purification of Single-walled Carbon Nanotubes Grown by a Chemical Vapour Deposition (CVD) Method
Authors:Cigang Xu  Emmanuel Flahaut  Sam R Bailey  Gareth Brown  Jeremy Sloan  Karl S Coleman  V Clifford Williams  Malcolm L H Green
Institution:1. Inorganic Chemistry Laboratory, University of Oxford, Oxford, OX1 3QR, UK;
2. Department of Materials, University of Oxford, Ocford, OX1 3PH, UK
Abstract:A procedure for purification of single walled carbon nanotubes(SWNTs) grown by the chemical vapour deposition(CVD) of carbon monooxide has been developed. Based on the result from TGA/DTA of as prepared sample, the oxidation temperature was determined. The process included sonication, oxidation and acid washing steps. The purity and yield after purification were determined and estimated by TEM. Moreover, for the first time, a loop structure for CVD SWNTs has been observed.
Keywords:Single  walled carbon nanotubes(SWNTs)  Purification  Chemical vapour deposition(CVD)
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