| 液相色谱-电喷雾质谱联用研究不同产地吴茱萸中生物碱成分 |
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| 引用本文： | 张雪琴,周欣,王道平,郝小江.液相色谱-电喷雾质谱联用研究不同产地吴茱萸中生物碱成分[J].分析化学,2005,33(2):241-244. |
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| 作者姓名： | 张雪琴 周欣 王道平 郝小江 |
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| 作者单位： | 中国科学院天然产物化学重点实验室,贵阳,550002;贵州大学精细化工中心,贵阳,550025;中国科学院天然产物化学重点实验室,贵阳,550002;中国科学院天然产物化学重点实验室,贵阳,550002;中国科学院昆明植物研究所,昆明,650204 |
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| 摘 要： | 采用液相色谱．电喷雾串联质谱分离鉴定了吴茱萸药材中5种生物碱成分。分析比较了不同产地吴茱萸药材中生物碱的种类，同时采用高效液相色谱测定了不同产地药材中吴茱萸次碱的含量。方法简单，快速。灵敏，结果令人满意。
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| 关 键 词： | 高效液相色谱 液相色谱-质谱联用 吴茱萸碱 吴茱萸次碱 羟基吴茱萸碱 吴茱萸酰胺甲 吴茱萸酰胺 |
Analysis of Alkaloids in Evodia Rutaecarpa from Different Habitats by Liquid Chroamtography/Mass Spectrometry |
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| Zhang Xueqin,Zhou Xin,Wang Daoping,Hao Xiaojiang.Analysis of Alkaloids in Evodia Rutaecarpa from Different Habitats by Liquid Chroamtography/Mass Spectrometry[J].Chinese Journal of Analytical Chemistry,2005,33(2):241-244. |
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| Authors: | Zhang Xueqin Zhou Xin Wang Daoping Hao Xiaojiang |
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| Abstract: | A liquid chromatography-electrospray ionization (ESI) tandem mass spectrometry was used to separate and identify five alkaloids in Evodia rutaecarpa. The type and content of alkaloids in Evodia rutaecarpa from nine different habitats were analysed and compared. The quantitations of rutaecarpine in Evodia rutaecarpa from nine different habitats were also performed by high performance liquid chromatography. The method is simple, quick and sensitive, the result is satisfactary. |
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