| 肉苁蓉挥发性化学成分分析 |
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| 引用本文： | 回瑞华,侯冬岩,李铁纯,关崇新.肉苁蓉挥发性化学成分分析[J].分析化学,2003,31(5):601-603. |
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| 作者姓名： | 回瑞华 侯冬岩 李铁纯 关崇新 |
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| 作者单位： | 鞍山师范学院分析测试研究中心,鞍山,114005 |
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| 基金项目： | 辽宁省教育厅科学技术基金资助课题(No.20331079) |
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| 摘 要： | 报道了用同时蒸馏—萃取法提取肉苁蓉挥发性物质，测得肉苁蓉挥发油的含量为3．5％；利用GC／MS法分离确认出24种化学成分；用峰面积归一化法得出各化学成分在挥发油中的相对百分含量，其中主要成分为丁香酚，占总挥发油的83．60％；又用单离子法分离出丁香酚，并用IR，EI-MS法对其进行分析确认。
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| 关 键 词： | 肉苁蓉 挥发性成分 蒸馏 萃取 丁香酚 中药 分析 |
Analysis of Volatile Components in Herba Cistanches |
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| Hui Ruihua,Hou Dongyan,Li Tiechun,Cuan Chongxin.Analysis of Volatile Components in Herba Cistanches[J].Chinese Journal of Analytical Chemistry,2003,31(5):601-603. |
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| Authors: | Hui Ruihua Hou Dongyan Li Tiechun Cuan Chongxin |
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| Abstract: | The volatile components of Herba Cistanches were extracted by simultaneous distillation-extraction method and analyzed by combined capillary gas chromatography/mass speetrometry. Among 24 identified compounds the eugenol was mainly component. The relative content of eugenol was 83.60% in the all volatile components detected. The eugenol was isolated by single-ion method and identified by infrared spectrscopy and mass spectrometry. |
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| Keywords: | Herba Cistanches volatile components simultaneous distillation-extraction eugenol |
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