| 液相色谱串联质谱法测定牛组织中氨丙啉残留量 |
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| 引用本文： | 李存,江潇潇,吴银良,皇甫伟国.液相色谱串联质谱法测定牛组织中氨丙啉残留量[J].分析化学,2011,39(4):576-579. |
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| 作者姓名： | 李存 江潇潇 吴银良 皇甫伟国 |
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| 作者单位： | 河北工程大学农学院;农业部农产品质量安全监督检验测试中心(宁波); |
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| 基金项目： | 宁波市自然科学基金(No.2009A610183); 宁波市农科院院长基金(No.09-12)资助项目 |
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| 摘 要： | 建立了牛组织中氨丙咻残留量的液相色谱串联质谱测定方法.样品经磷酸盐缓冲液提取后用HLB小柱净化,甲醇洗脱,洗脱液氮吹后用0.1%甲酸-甲醇(90:10,V/V)溶解,进行LC-MS/MS分析.采用XBridge<'TM> C<,18>色谱柱分离,用0.1%甲酸-甲醇(90:10,V/V)作为流动相等度洗脱,电喷雾正离子...
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| 关 键 词： | 氨丙啉 液相色谱串联质谱法 牛组织 残留 |
Determination of Amprolium Residues in Bovine Tissues by Liquid Chromatography with Tandem Mass Spectrometry |
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| LI Cun,JIANG Xiao-Xiao,WU Yin-Liang,HUANGFU Wei-Guo.Determination of Amprolium Residues in Bovine Tissues by Liquid Chromatography with Tandem Mass Spectrometry[J].Chinese Journal of Analytical Chemistry,2011,39(4):576-579. |
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| Authors: | LI Cun JIANG Xiao-Xiao WU Yin-Liang HUANGFU Wei-Guo |
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| Institution: | LI Cun1,JIANG Xiao-Xiao2,WU Yin-Liang2,HUANGFU Wei-Guo2 1(College of Agriculture,Hebei University of Engineering,Handan 056038)2(The Supervision,Inspection & Testing Center of Agricultural Products Quality & Security(Ningbo),Ministry of Agriculture,Ningbo 315040) |
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| Abstract: | |
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| Keywords: | Amprolium Liquid chromatography with tandem mass spectrometry Bovine tissues Residue |
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