| 悬浮液进样电感藕合等离子体发射光谱中颗粒的输运和蒸发行为 |
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| 引用本文： | 张军烨,汪正,杜一平,邱德仁,杨芃原.悬浮液进样电感藕合等离子体发射光谱中颗粒的输运和蒸发行为[J].分析化学,2011,39(5):658-663. |
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| 作者姓名： | 张军烨 汪正 杜一平 邱德仁 杨芃原 |
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| 作者单位： | 张军烨,ZHANG Jun-Ye(华东理工大学,化学与分子工程学院,上海,200237;中国科学院上海硅酸盐研究所,上海,200050);汪正,WANG Zheng(中国科学院上海硅酸盐研究所,上海,200050);杜一平,DU Yi-Ping(华东理工大学,化学与分子工程学院,上海,200237);邱德仁,杨芃原
,QIU De-Ren,YANG Peng-Yuan(复旦大学化学系,上海,200433) |
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| 基金项目： | 国家自然科学基金资助项目，中科院上海硅酸盐所科技创新项目 |
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| 摘 要： | 以碳化硼为例,研究了悬浮液雾化进样中的粒子在传输和蒸发过程中的行为,并对分析结果出现负偏离的原因进行了详细探讨.对比悬浮液颗粒的原始粒径分布和经过传输过程后的粒径分布,获得到达等离子体的颗粒粒径上限小于10 Am.样品中存在的部分超大粒径的颗粒(d>>10 μm)会严重影响可传输区域颗粒(d<10 μm)的质量运输效率...
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| 关 键 词： | 碳化硼 悬浮液雾化进样 电感耦合等离子体光谱 负偏离 |
Transportation and Evaporation Behavior of Suspension Particle for Slurry Nebulization Introduction in Inductively Coupled Plasma Optical Emission Spectrometry |
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| ZHANG Jun-Ye,WANG Zheng,DU Yi-Ping,QIU De-Ren,YANG Peng-Yuan.Transportation and Evaporation Behavior of Suspension Particle for Slurry Nebulization Introduction in Inductively Coupled Plasma Optical Emission Spectrometry[J].Chinese Journal of Analytical Chemistry,2011,39(5):658-663. |
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| Authors: | ZHANG Jun-Ye WANG Zheng DU Yi-Ping QIU De-Ren YANG Peng-Yuan |
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| Institution: | ZHANG Jun-Ye1,2,WANG Zheng2,DU Yi-Ping1,QIU De-Ren3,YANG Peng-Yuan3 1(Shanghai Institute of Ceramics,Chinese Academy of Sciences,Shanghai 200050) 2(School of Chemistry and Molecular Engineering,East China University of Science and Technology,Shanghai 200037) 3(Department of Chemistry,Fudan University,Shanghai 200433) |
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| Abstract: | The behavior of boron carbide slurry particles in the transportation process and vaporization process of suspension nebulization inductively coupled plasma optical emission spectrometry(ICP-OES) was investigated to study how the negative deviation in the determination results of advanced ceramic materials by using slurry nebulization ICP-OES with aqueous standards calibration came into being.Both the particle size distribution of the original ceramic powders and the particle size distribution after pneumati... |
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| Keywords: | Boron carbide Slurry nebulization Inductively coupled plasma emission spectrometry Negative deviation |
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