| 8-氨基喹啉-5-位偶氮衍生物的合成及其与钯的显色反应比较研究 |
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| 引用本文： | 赵建为,徐其亨.8-氨基喹啉-5-位偶氮衍生物的合成及其与钯的显色反应比较研究[J].分析化学,1992(6). |
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| 作者姓名： | 赵建为 徐其亨 |
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| 作者单位： | 云南大学化学系，云南大学化学系 昆明 650091 昆明冶金研究所，昆明 650091 |
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| 摘 要： | 以8-氨基喹啉为母体合成了19个5-位偶氮衍生物,其中14个是新化合物。系统研究它们与钯的显色反应,发现了试剂取代结构对试剂及其络合物光度特性的影响规律。初步研究了MOPAQ及AAPAQ光度测钯的新体系,并与PAQ比较,诸条件得到改善。
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| 关 键 词： | 8-氨基喹啉-5-位偶氮衍生物 显色反应 钯 |
Synthesis of 8-Aminoquinoline-5-post Azo Derivatives and Comparison of Their Color Reactions With Palladium |
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| Zhao Jianwei,Xu Qiheng.Synthesis of 8-Aminoquinoline-5-post Azo Derivatives and Comparison of Their Color Reactions With Palladium[J].Chinese Journal of Analytical Chemistry,1992(6). |
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| Authors: | Zhao Jianwei Xu Qiheng |
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| Abstract: | Nineteen 8-aminoquinoline-5-post azo derivatives are synthesized, and fourteen of them is new compounds. Their color reactions with palladium were studied. The law of effects of substitute groups was found. Two new systems for the spectrophotometric determination of palladium with 5-(4-acetylaminophenylazo)-8-aminoquinoline and 5-(4-methoxyphenylazo)-8-aminoquinoline has been developed, and their conditions were better than those of phenylazo-8-aminoquinoline. |
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| Keywords: | 8-Aminoquinolinc-5-post azo derivatives Color reaction Palladium |
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