| 高效液相色谱电喷雾质谱快速鉴定粉葛中C-苷及O-苷同分异构体 |
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| 引用本文： | 周安,孙晓娟,吴虹,李庆林,吴鸿飞.高效液相色谱电喷雾质谱快速鉴定粉葛中C-苷及O-苷同分异构体[J].分析化学,2012,40(4):612-616. |
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| 作者姓名： | 周安 孙晓娟 吴虹 李庆林 吴鸿飞 |
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| 作者单位： | 1. 安徽中医学院,合肥230038;安徽省现代中药研究与开发重点实验室,合肥230038
2. 赛默飞世尔科技(中国)有限公司,上海,201206 |
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| 摘 要： | 采用高效液相色谱(二极管阵列)/电喷雾质谱联用系统( HPLC-PDA-ESI-MSn)快速鉴定中药粉葛中C-苷及O-苷异黄酮同分异构体.选用Hypersil Gold C18(150 mm×2.1 mm×3 μm)色谱柱,以水(含0.1％甲酸)-乙腈为流动相进行梯度洗脱,研究了粉葛中11种异黄酮类化合物的正离子一级、...
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| 关 键 词： | 粉葛 高效液相色谱-电喷雾质谱 同分异构体 源内碰撞诱导解离 |
Rapid Identified C-Glycosides and Their Isomer O-Glycosides in Radix Puerariae Thomsonii Using High Performance Liquid Chromatography-Photo Diode Array-Electrospray Ionization Tandem Mass Spectrometry |
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| ZHOU An
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SUN Xiao-Juan
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WU Hong
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LI Qing-Lin
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WU Hong-Fei.Rapid Identified C-Glycosides and Their Isomer O-Glycosides in Radix Puerariae Thomsonii Using High Performance Liquid Chromatography-Photo Diode Array-Electrospray Ionization Tandem Mass Spectrometry[J].Chinese Journal of Analytical Chemistry,2012,40(4):612-616. |
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| Authors: | ZHOU An SUN Xiao-Juan WU Hong LI Qing-Lin WU Hong-Fei |
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| Institution: | 1,2 1(Anhui University of Traditional Chinese Medicine,Hefei 230038,China) 2(Anhui Province Key Laboratory of R&D of Chinese Medicine,Hefei 230038,China) 3(Thermo Fisher Scientific,Shanghai 201206,China) |
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