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均匀共沉淀-水热法制备纤维状羟基磷酸钙/壳聚糖复合粉体
引用本文:杨洪,宁黔冀,赵海涛. 均匀共沉淀-水热法制备纤维状羟基磷酸钙/壳聚糖复合粉体[J]. 化学研究与应用, 2005, 17(2): 186-189
作者姓名:杨洪  宁黔冀  赵海涛
作者单位:河南师范大学生命科学学院,河南,新乡,453002
基金项目:河南省自然科学基金项目 (0 4110 3 190 0 ),河南省教育厅自然科学研究计划(2 0 0 460 10 74),河南省师范大学青年基金资助(2 0 0 15 2 10 3 9)
摘    要:以尿素沉淀剂,运用溶液均匀共沉淀法制得纤维状羟基磷灰石(HAP)和无定形颗粒状守壳聚糖(CS)的复合粉体,通过水势处理调整纤维状HAP晶粒尺寸的大小,对粉体进行了XRD、TEM、IR及化学组成(Ca/P)表征。均匀一水热共沉淀过程中,pH值对粉体Ca/P、XRD、TEM、IR有很大影响。

关 键 词:壳聚糖 羟基磷酸钙 均匀-水热共沉淀
文章编号:1004-1656(2005)02-0186-04
修稿时间:2004-03-31

Preparition of hydroxypatite/chitosan composited powder with hoogeneous co-precipitation-hydrothermal method
YANG Hong,NING Qian-ji,ZHAO Hai-tao. Preparition of hydroxypatite/chitosan composited powder with hoogeneous co-precipitation-hydrothermal method[J]. Chemical Research and Application, 2005, 17(2): 186-189
Authors:YANG Hong  NING Qian-ji  ZHAO Hai-tao
Abstract:Using urea as the precipitant,the fibrous hydroxypatite(HAP)/chitosan (CS)composited powder was prepared with homogeneous co-oprecipitation,and the grain size of HAP was adjusted with hydrothermal treating(0.2MPa).The composited powder was characterrised by XRD,TEM and IR and chemical composition(Ca/P).In the course of homogeneous-hydrothermal co-precipitating,the pH value had great influence on Ca/P,XRD,TEM,and IR.
Keywords:chitosan  hydroxyapatite  homogeneous-hydrothermal  co-precipitation
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