| 阻燃抗氧剂9,10-二氢-9-氧杂-10-膦菲-10-氧的合成 |
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| 引用本文： | 赵小平,李绍文,杨军,丁向东,尤裕如.阻燃抗氧剂9,10-二氢-9-氧杂-10-膦菲-10-氧的合成[J].化学研究与应用,2000,12(6):648-650. |
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| 作者姓名： | 赵小平 李绍文 杨军 丁向东 尤裕如 |
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| 作者单位： | 安徽省化工研究院,安徽,合肥,230041 |
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| 摘 要： | Phenylphenol,phosphorus trichloride and aluminium trichloride were mixed and rea cted between 60～215℃ for about 11h,then vacuum-distill ed at 202～235℃ under pressure of -750mmHg.The distillate was added to sodium c arbonate solution for hydrolysis.The product was then crystallized by acid,filte red,dried.Vacuum-dehydration reaction and grinding were followed to give the ti tle product.
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| 关 键 词： | 阻燃抗氧剂 合成 POP 芳烃 酰基化反应 |
| 修稿时间： | 1999-12-06 |
SYNTHESIS OF FLAME RETARDANT AND ANTIOXIDANT 9,10-DIHYDRO-9-OXA-10-PHOSPHAPHENANTHRENE-10-OXIDE(POP) |
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| ZHAO Xiao-ping,LI Shao-wen,YANG Jun,DING Xiang-dong,YOU Yu-ru.SYNTHESIS OF FLAME RETARDANT AND ANTIOXIDANT 9,10-DIHYDRO-9-OXA-10-PHOSPHAPHENANTHRENE-10-OXIDE(POP)[J].Chemical Research and Application,2000,12(6):648-650. |
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| Authors: | ZHAO Xiao-ping LI Shao-wen YANG Jun DING Xiang-dong YOU Yu-ru |
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| Abstract: | Phenylphenol,phosphorus trichloride and aluminium trichloride were mixed and rea cted between 60～215℃ for about 11h,then vacuum-distill ed at 202～235℃ under pressure of -750mmHg.The distillate was added to sodium c arbonate solution for hydrolysis.The product was then crystallized by acid,filte red,dried.Vacuum-dehydration reaction and grinding were followed to give the ti tle product. |
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| Keywords: | flame retardant and antioxidant 9 10-dihydro-9 -oxa-10-phosphaphenanthrene-10-oxide synthesis o-phenylphenol |
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