| 微波辐射下4,6-二羟基嘧啶与醛的反应研究 |
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| 引用本文： | 唐自强,徐佳宁,屠树江,陈艳,姜波,贾润红.微波辐射下4,6-二羟基嘧啶与醛的反应研究[J].有机化学,2008,28(3):440-442. |
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| 作者姓名： | 唐自强 徐佳宁 屠树江 陈艳 姜波 贾润红 |
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| 作者单位： | 1. 徐州工程学院化学化工学院,徐州,221006
2. 徐州师范大学化学化工学院,徐州,221116 |
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| 基金项目： | 国家自然科学基金，江苏省自然科学基金，江苏省六大人才高峰基金，徐州工程学院重点研究课题 |
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| 摘 要： | 以甲胺为催化剂、醋酸为溶剂, 微波促进下芳香醛与两分子4,6-二羟基嘧啶反应得到6-羟基-5-(4-羟基-6-氧代-1,6-二氢嘧啶-5-基)芳甲基]嘧啶-4(3H)-酮衍生物.
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| 关 键 词： | 微波辐射 4 6-二羟基嘧啶 双嘧啶 |
| 收稿时间： | 2007-04-19 |
| 修稿时间： | 2007-08-25 |
Reaction of Pyrimidine-4,6-diol with Aldehydes under Microwave Irradiation |
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| TANG Zi-Qiang,XU Jia-Ning,TU Shu-Jiang,CHEN Yan,JIANG Bo,JIA Run-Hong.Reaction of Pyrimidine-4,6-diol with Aldehydes under Microwave Irradiation[J].Chinese Journal of Organic Chemistry,2008,28(3):440-442. |
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| Authors: | TANG Zi-Qiang XU Jia-Ning TU Shu-Jiang CHEN Yan JIANG Bo JIA Run-Hong |
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| Institution: | (School of Chemistry and Chemical Engineering, Xuzhou Institute of Technology, Xuzhou 221006)( School of Chemistry and Chemical Engineering, Xuzhou Normal Univer-sity, Xuzhou 221116) |
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| Abstract: | The reaction of double equivalent pyrimidine-4,6-diol with aldehydes afforded 6-hydroxy-5-(4-hydroxy-6-oxo-1,6-dihydropyrimidin-5-yl)arymethyl]pyrimidin-4(3H)-one deriva-tives under microwave irradiation using methylamine as a catalyst and acetic acid as a solvent. |
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| Keywords: | microwave irradiation pyrimidine-4 6-diol bipyrimidine |
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