| 微波辐射条件下季戊四醇双缩醛和双缩酮化合物的合成 |
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| 引用本文： | 靳通收,张伏生,王开芳,李同双.微波辐射条件下季戊四醇双缩醛和双缩酮化合物的合成[J].有机化学,2004,24(11):1485-1488. |
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| 作者姓名： | 靳通收 张伏生 王开芳 李同双 |
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| 作者单位： | 河北大学化学与环境科学学院,保定,071002 |
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| 基金项目： | 国家自然科学基金，教育部高校骨干教师资助计划，河北省教育厅科研项目 |
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| 摘 要： | 微波辐射硫酸锆-硅胶催化季戊四醇与醛、酮缩合反应,高收率制得了双缩醛和双缩酮化合物.该方法操作简便,收率高,催化剂可重复使用,是一种环境友好型催化反应.
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| 关 键 词： | 微波 双缩醛(酮) 季戊四醇 醛 酮 合成 |
| 修稿时间： | 2004年4月27日 |
Synthesis of Pentaerythritol Diacetals from Aldehydes and Ketones under Microwave Irradiation |
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| JIN,Tong-Shou ZHANG,Fu-Sheng WANG,Kai-Fang LI,Tong-Shuang.Synthesis of Pentaerythritol Diacetals from Aldehydes and Ketones under Microwave Irradiation[J].Chinese Journal of Organic Chemistry,2004,24(11):1485-1488. |
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| Authors: | JIN Tong-Shou ZHANG Fu-Sheng WANG Kai-Fang LI Tong-Shuang |
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| Abstract: | The pentaerythritol diacetals were effectively synthesized through condensation reaction of pentaerythritol with aldehydes and ketones promoted by zirconium sulfate-silica gel under microwave irradiation. The easy procedure provided a neat environment-friendly synthetic method for pentaerythritol diacetals in high yields and the catalyst was reusable. |
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| Keywords: | microwave diacetal pentaerythritol aldehyde ketone synthesis |
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