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| N,N-二取代甘氨酸四乙酰基葡萄糖酯的合成与表征 | |
| 引用本文： | 李英俊,刘军,许永廷,靳煜,孙淑琴,丁万刚,刘丽军.N,N-二取代甘氨酸四乙酰基葡萄糖酯的合成与表征[J].有机化学,2009,29(2):302-306. |
| 作者姓名： | 李英俊 刘军 许永廷 靳煜 孙淑琴 丁万刚 刘丽军 |
| 作者单位： | 1. 辽宁师范大学化学化工学院,大连,116029 2. 大连理工大学精细化工国家重点实验室,大连,116012 |
| 摘 要： | 在碳酸钾和十六烷基三甲基溴化铵存在下, 将N-(N-乙酰基-N-芳氨基乙酰基)-N-芳氨基乙酸与全乙酰化α-溴代葡萄糖反应合成出了7个新的N,N-二取代甘氨酸四乙酰基葡萄糖酯(5a～5g), 并利用IR, 1H NMR, MS和元素分析对其结构进行了表征. |
| 关 键 词： | 全乙酰化葡萄糖酯 N-(N-乙酰基-N-芳氨基乙酰基)-N-芳氨基乙酸 合成 表征 |
| 收稿时间： | 2008-6-30 |
| 修稿时间： | 2008-10-29 |
Synthesis and Characterization of N,N-Disubstituted Glycine Tetraacetyl Glucosyl Esters |
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| Li Yingjun,Liu Jun,Xu Yongting,Jin Kun,Sun Shuqin,Ding Wangang,Liu Lijun.Synthesis and Characterization of N,N-Disubstituted Glycine Tetraacetyl Glucosyl Esters[J].Chinese Journal of Organic Chemistry,2009,29(2):302-306. | |
| Authors: | Li Yingjun Liu Jun Xu Yongting Jin Kun Sun Shuqin Ding Wangang Liu Lijun |
| Institution: | (a College of Chemistry and Chemical Engineering, Liaoning Normal University, Dalian 116029) (b State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian 116012) |
| Abstract: | Seven new N,N-disubstituted glycine tetraacetyl glucosyl esters (5a～5g) were synthesized by the reaction of N-(N-acetyl-N-arylglycyl)-N-arylglycines with 2,3,4,6-tetra-O-acetyl-α-D-glucopyransoyl bromide in the presence of hexadecyltrimethyl ammonium bromide and potassium carbonate. The structures of the target compounds were characterized by IR, 1H NMR, MS techniques and elemental analysis. |
| Keywords: | per-acetylated glucosyl ester N-(N-acetyl-N-arylglycyl)-N-arylglycine synthesis characteriza-tion |
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