《有机化学》1989年索引

产率23‘8%。m.p.91~93℃。C,。H,3NS,计算值:C,78.51;H,4.76;N,5.09;s,z一64、。实测值:C,78.76;H, 4.85;N,4.61;S,11.78。v二.二:3020,1590,1500,1470,1450,770,750,700 em一‘。乃,工:6.1了一7.46(m)Ppm。N一(2一毗咤蓦)吩嚷峰(3b) LO.Og Za,8.29 ld,80mL CoHoN02,7.09无水K:C03,1.09 Cu粉,反应12h,粗产物用硅胶柱层析分离。产率:29.7%。m.p一02~104℃。C17H::N:S,计算值:C,73.89;H,4.37;N,10.13;S,11.60。实测值:C,73.85;H,4,IB;N,9.96;S,1 2 .01。voa二:3050,3010,1600,1490,1470,1430,770,750,710 em一’。6H:6.76一8…