| 2,5-二取代-1,3,4-三唑的合成 |
| |
| 引用本文： | 雷茂义,邹建平,饶卫东.2,5-二取代-1,3,4-三唑的合成[J].有机化学,2006,26(7):1001-1003. |
| |
| 作者姓名： | 雷茂义 邹建平 饶卫东 |
| |
| 作者单位： | 苏州大学化学化工学院江苏省有机合成重点实验室,苏州,215006 |
| |
| 基金项目： | 江苏省有机合成重点实验室(No.JSK016)资助项目. |
| |
| 摘 要： | 以苯甲酰氯、硫氰酸钾和芳胺为起始原料, 合成了1-苯甲酰基-3-芳基硫脲1a～1g, 再与水合肼反应合成了2,5-二取代-1,3,4-三唑2a～2g. 化合物2的结构经IR, 1H NMR和HRMS确证.
|
| 关 键 词： | 1-苯甲酰基-3-芳基硫脲 2 5-二取代-1 3 4-三唑 合成 |
| 收稿时间： | 06 30 2005 12:00AM |
| 修稿时间： | 01 25 2006 12:00AM |
Synthesis of 2,5-Disubstituted-1,3,4-triazole Derivatives |
| |
| LEI Mao-Yi,ZOU Jian-Ping,RAO Wei-Dong.Synthesis of 2,5-Disubstituted-1,3,4-triazole Derivatives[J].Chinese Journal of Organic Chemistry,2006,26(7):1001-1003. |
| |
| Authors: | LEI Mao-Yi ZOU Jian-Ping RAO Wei-Dong |
| |
| Institution: | Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry and Chemical Engineering, Suzhou University, Suzhou 215006 |
| |
| Abstract: | 2,5-Disubstituted-1,3,4-triazole derivatives were prepared by the reaction of hydrazine hydrate with 1-benzoyl-3-arylthioureas obtained from the reaction of benzoyl chloride, potassium thiocyanate and aniline, and their structures were confirmed by IR, 1H NMR and HRMS spectra. |
| |
| Keywords: | 1-benzoyl-3-arylthiourea 2 5-disubstituted-1 3 4-triazole synthesis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
| 点击此处可从《有机化学》浏览原始摘要信息 |
| 点击此处可从《有机化学》下载免费的PDF全文 |
|
