| 含三唑基的新型咪唑[2,1-b]-1,3,4-噻二唑的合成及表征 |
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| 引用本文： | 崔蕾,陈家胜,刘方明,解正峰,孙亚栋,王厚勇.含三唑基的新型咪唑[2,1-b]-1,3,4-噻二唑的合成及表征[J].有机化学,2006,26(7):963-966. |
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| 作者姓名： | 崔蕾 陈家胜 刘方明 解正峰 孙亚栋 王厚勇 |
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| 作者单位： | 1. 新疆大学化学化工学院,乌鲁木齐,830046
2. 新疆大学化学化工学院,乌鲁木齐,830046;杭州师范学院化学系,杭州,310012;杭州师范学院有机硅化学及材料技术教育部重点实验室,杭州,310012 |
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| 基金项目： | 国家自然科学基金(Nos.29702007,20162004)资助项目. |
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| 摘 要： | 以2-(2-苯基-1,2,3-三唑-4-基)-5-氨基-1,3,4-噻二唑(1)为原料分别与ω-溴代芳基乙酮、ω-溴代-ω-(1H-1,2,4-三唑-1-基)芳基乙酮反应, 合成了一系列新型咪唑2,1-b]-1,3,4-噻二唑类化合物2a～2e和3a～3e. 其结构经IR, 1H NMR和MS及元素分析确证.
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| 关 键 词： | 1 2 3-三唑 1 2 4-三唑 咪唑[2 1-b]-1 3 4-噻二唑 |
| 收稿时间： | 05 18 2005 12:00AM |
| 修稿时间： | 01 25 2006 12:00AM |
Synthesis and Characterization of New Imidazolo[2,1-b]-1,3,4- thiadiazoles Containing Triazole |
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| CUI Lei,CHEN Jia-Sheng,LIU Fang-Ming,XIE Zheng-Feng,SUN Ya-Dong,WANG Hou-Yong.Synthesis and Characterization of New Imidazolo[2,1-b]-1,3,4- thiadiazoles Containing Triazole[J].Chinese Journal of Organic Chemistry,2006,26(7):963-966. |
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| Authors: | CUI Lei CHEN Jia-Sheng LIU Fang-Ming XIE Zheng-Feng SUN Ya-Dong WANG Hou-Yong |
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| Institution: | 1. College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046;2. Department of Chemistry, Hangzhou Teaching College, Hangzhou 310012; 3. Key Laboratory of Organosilicon Chemistry and Material Technology, Ministry of Education, Hangzhou Teaching College, Hangzhou 310012 |
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| Abstract: | A series of imidazolo2,1-b]-1,3,4-thiadiazoles were synthesized by the reaction of 2-(2-phenyl- 1,2,3-triazol-4-yl)-5-amino-1,3,4-thiadiazole with ω-bromoacetophenones or ω-bromo-ω-(1H-1,2,4-triazol- 1-yl)acetophenones in reflux EtOH. Their structures were characterized by elemental analysis, IR, 1H NMR and MS spectra. |
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| Keywords: | 1 2 3-triazole 1 2 4-triazole imidazolo[2 1-b]-1 3 4-thiadiazole |
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