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Structural Peculiarities of Anomalous Electrolytic Palladium Deposits Prepared under Hydride Formation Conditions |
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| Authors: | Roginskaya Yu E Lubnin E N Safonova T Ya Chuvilin A L Politova E D Tsirlina G A |
| Institution: | (1) Russian Federation Scientific Center,  Karpov Research Institute of Physical Chemistry, , ul. Vorontsovo pole 10, Moscow, 105064, Russia;(2) Moscow State University, Vorob'evy gory 1, Moscow, 119899, Russia;(3) Boreskov Institute of Catalysis, Siberian Division, Russian Academy of Sciences, pr. Akademika Lavrent'eva 5, Novosibirsk, 630090, Russia |
| Abstract: | The peculiarities of bulk and surface structures of electrolytic palladium deposits formed under hydride formation conditions are studied by x-ray diffraction (XRD) and x-ray photoelectron spectroscopy techniques. For anomalous deposits with high hydrogen capacities, the evolution of the XRD behavior is traced as a function of thermal treatment. The material is shown to comprise two cubic phases with different lattice parameters. |
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