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极谱法测定蒙药那如三味丸中锗的研究
引用本文:赵丹庆,孙占才,张力.极谱法测定蒙药那如三味丸中锗的研究[J].广东微量元素科学,2011,18(2):51-52.
作者姓名:赵丹庆  孙占才  张力
作者单位:内蒙古民族大学化学化工学院,内蒙,通辽,028042
摘    要:采用差分脉冲极谱法,在pH 1.50、含3,4 –二羟基苯甲醛(DHB)的H2SO4中,测得无机锗的峰电位为Ep=-0.54 V,Ge(Ⅳ)浓度在1.04×10 5~1.05×10 4 mol·L 1范围内与峰电流呈线性关系,利用该法用于测定蒙药那如三味丸中总锗、无机锗和有机锗,得到了满意的结果.

关 键 词:差分脉冲极谱法    蒙药

Determination of Germanium in Mongolia Medicine Naru Sanwei Pill by Polarography
ZHAO Danqing,SUN Zhancai,ZHANG Li.Determination of Germanium in Mongolia Medicine Naru Sanwei Pill by Polarography[J].Trace Elements Science,2011,18(2):51-52.
Authors:ZHAO Danqing  SUN Zhancai  ZHANG Li
Institution:( College of Chemistry and Chemical Engineering , Inner Mongolia University for Nationalities, Inner Mongolia Tongliao 028042, China)
Abstract:The amount of Ge( Ⅳ ) in pH 1.30 H2SO4 including 3,4 - dihydroxy benzaldehyde supporting electrolyte was determined by differential pulse polarography. The peak potential is located at Ep = - 0. 54 V with peak current proportional to concentration of Ge ( Ⅳ ) in 1.04 × 10^-5 - 1.05 × 10^-4 mol · L^-1 This method was applied to the determination of total germanium, organic germanium and inorganic germanium in Mongolia medicine Naru Sanwei pill with satisfactory results.
Keywords:differential pulse polarography  germanium  Mongolia medicine
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