| 碱式碳酸锌煅烧制备纳米氧化锌 |
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| 引用本文： | 张宪玺,王晓娟,翟冠杰,姜建壮.碱式碳酸锌煅烧制备纳米氧化锌[J].无机化学学报,2002,18(10):1037-1041. |
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| 作者姓名： | 张宪玺 王晓娟 翟冠杰 姜建壮 |
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| 作者单位： | 山东大学化学与化工学院,济南,250100 |
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| 基金项目： | 国家自然科学基金资助项目(No.20171028)，国家科技部973项目(No.2001CB6105-04，2001CB6105-06)，山东省自然科学基金资助项目(No.Z99B03，Y2001B05)。 |
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| 摘 要： | The reaction process of nanometer ZnO preparation through basic zinc carbonate calcination was investigated via TG-DTG-DTA, IR, XRD and TEM methods. The spectra features and morphology variations of precursor and target products calcinated at different temperatures were investigated. The reaction process was deduced to be three stages, which include breaking of precursor crystallites, their decomposition, and growth of ZnO crystal nucleus. The most appropriate temperature for this reaction was demonstrated to be about 300℃.
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| 关 键 词： | 纳米 氧化锌 煅烧 过程分析 |
| 修稿时间： | 2002年5月15日 |
Nanometer ZnO Preparation through Basic Zinc Carbonate Calcination |
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| ZHANG Xian-Xi,WANG Xiao-Juan,ZHAI Guan-Jie and JIANG Jian-Zhuang.Nanometer ZnO Preparation through Basic Zinc Carbonate Calcination[J].Chinese Journal of Inorganic Chemistry,2002,18(10):1037-1041. |
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| Authors: | ZHANG Xian-Xi WANG Xiao-Juan ZHAI Guan-Jie and JIANG Jian-Zhuang |
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| Institution: | School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100,School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100,School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100 and School of Chemistry and Chemical Engineering, Shandong University, Jinan 250100 |
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| Abstract: | |
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| Keywords: | nanometer zinc oxide calcination process analysis |
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