| 纳米CuO：不同形貌的制备及对高氯酸铵热分解催化性能 |
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| 引用本文： | 衡秋丽,肖 峰,骆建敏,孙庆军,王吉德,宿新泰.纳米CuO：不同形貌的制备及对高氯酸铵热分解催化性能[J].无机化学学报,2009,25(2):359-363. |
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| 作者姓名： | 衡秋丽 肖 峰 骆建敏 孙庆军 王吉德 宿新泰 |
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| 作者单位： | 新疆大学化学化工学院,石油天然气教育部重点实验室,乌鲁木齐,830046 |
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| 基金项目： | 新疆大学博士毕业生启动基金，新疆维吾尔自治区科技攻关重大专项项目 |
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| 摘 要： | 采用超声法和微波水热法，制备了棒状、球状、梭形和杨桃状纳米CuO粉体。以X-射线粉末衍射仪(XRD)、透射电镜(TEM)手段对各种产物进行了表征。用热分析法考察了不同形貌的纳米CuO对高氯酸铵(AP)分解的催化作用。结果表明，四种形貌的纳米CuO均可强烈催化AP的热分解，而棒状和球状纳米CuO的催化活性更高。与纯高氯酸铵相比，加入棒状纳米CuO后AP的高温分解温度降低了124.4 ℃，加入球形纳米CuO催化剂后高温分解温度降低了122 ℃，且低温分解峰消失。
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| 关 键 词： | 纳米CuO 超声法 微波水热法 催化性能 高氯酸铵 |
Nano-CuO: Preparation with Different Morphologies and Catalytic Performance for Thermal Decomposition of Ammonium Perchlorate |
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| HENG Qiu-Li,XIAO Feng,LUO Jian-Min,SUN Qing-Jun,WANG Ji-De and SU Xin-Tai.Nano-CuO: Preparation with Different Morphologies and Catalytic Performance for Thermal Decomposition of Ammonium Perchlorate[J].Chinese Journal of Inorganic Chemistry,2009,25(2):359-363. |
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| Authors: | HENG Qiu-Li XIAO Feng LUO Jian-Min SUN Qing-Jun WANG Ji-De and SU Xin-Tai |
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| Institution: | College of Chemistry and Chemical Engineering, Xinjiang University, Key Laboratory of Oil and Gas Fine Chemicals, Educational Ministry of China, Urumqi 830046,College of Chemistry and Chemical Engineering, Xinjiang University, Key Laboratory of Oil and Gas Fine Chemicals, Educational Ministry of China, Urumqi 830046,College of Chemistry and Chemical Engineering, Xinjiang University, Key Laboratory of Oil and Gas Fine Chemicals, Educational Ministry of China, Urumqi 830046,College of Chemistry and Chemical Engineering, Xinjiang University, Key Laboratory of Oil and Gas Fine Chemicals, Educational Ministry of China, Urumqi 830046,College of Chemistry and Chemical Engineering, Xinjiang University, Key Laboratory of Oil and Gas Fine Chemicals, Educational Ministry of China, Urumqi 830046 and College of Chemistry and Chemical Engineering, Xinjiang University, Key Laboratory of Oil and Gas Fine Chemicals, Educational Ministry of China, Urumqi 830046 |
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| Abstract: | |
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| Keywords: | CuO nanopowders Ultrosonic method Microwave hydrothermal Catalytic property NH4ClO4 |
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