1,4-双(1′-苯基-3′-甲基-5′-氧代吡唑-4′-基)丁二酮-(1,4)合双铜(Ⅱ)配合物的合成、表征、非等温热分解反应动力学及电化学性质 |
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引用本文: | 单纯,贾殿赠,夏熙.1,4-双(1′-苯基-3′-甲基-5′-氧代吡唑-4′-基)丁二酮-(1,4)合双铜(Ⅱ)配合物的合成、表征、非等温热分解反应动力学及电化学性质[J].无机化学学报,1997,13(4):433-436. |
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作者姓名: | 单纯 贾殿赠 夏熙 |
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作者单位: | 新疆大学化学系,乌鲁木齐 830046,新疆大学化学系,乌鲁木齐 830046,新疆大学化学系,乌鲁木齐 830046 |
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摘 要: | The paper reported the synthetic procedure and character of Copper(Ⅱ) binuclear coordination compound of 1,4-bis-(1′-phenyl-3′-methyl-5′-pyrazolone-4′)-1,4-butanedione. The non-isothermal kinetic of the thermal decomposition of the complex has been studied from the TG-DTG curves by means of the Achar et al and Coats-Redfern methods. The electrochemical characterization of the complex were studied by means of powder microelectrodes technique.
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关 键 词: | β-二酮 双核配合物 非等温热分解 电化学性质 |
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