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水热法合成K0.5Bi0.5TiO3纳米陶瓷粉体
引用本文:侯磊,侯育冬,宋雪梅,朱满康,汪浩,严辉.水热法合成K0.5Bi0.5TiO3纳米陶瓷粉体[J].无机化学学报,2006,22(3):563-566.
作者姓名:侯磊  侯育冬  宋雪梅  朱满康  汪浩  严辉
作者单位:教育部新型功能材料重点实验室,北京工业大学材料科学与工程学院,北京,100022
基金项目:中国科学院资助项目;北京市"拔尖创新人才选拔计划"项目
摘    要:K0.5Bi0.5TiO3(KBT)nanocrystalline particles were hydrothermally synthesized from Bi(NO3)3·5H2O, TiO2 and KOH. The crystal phase, chemical composition and microstructure were characterized by XRD, XRF, Raman scattering spectroscopy and TEM. The results indicated that the products were pure perovskite structured K0.5Bi0.5TiO3 with chemical stoichiometry and perovskite structure. The TEM observation revealed that the particles possessed a feature of cubic shape and a nano-scale of about 40 nm. The KBT ceramics sintered at 1 040 ℃ from hydrothermal powders show higher density and better electric properties than that prepared by a solid-state reaction method.

关 键 词:水热法    钛酸铋钾    无铅压电陶瓷
文章编号:1001-4861(2006)03-0563-04
收稿时间:2005-09-26
修稿时间:2005-12-16

Hydrothermal Synthesis of K0.5Bi0.5TiO3 Lead-free Piezoelectric Ceramic
HOU Lei,HOU Yu-Dong,SONG Xue-Mei,ZHU Man-Kang,WANG Hao and YAN Hui.Hydrothermal Synthesis of K0.5Bi0.5TiO3 Lead-free Piezoelectric Ceramic[J].Chinese Journal of Inorganic Chemistry,2006,22(3):563-566.
Authors:HOU Lei  HOU Yu-Dong  SONG Xue-Mei  ZHU Man-Kang  WANG Hao and YAN Hui
Institution:Key Laboratory of Advanced Functional Materials of China Education Ministry, Department of Materials Science and Engineering, Beijing University of Technology, Beijing 100022,Key Laboratory of Advanced Functional Materials of China Education Ministry, Department of Materials Science and Engineering, Beijing University of Technology, Beijing 100022,Key Laboratory of Advanced Functional Materials of China Education Ministry, Department of Materials Science and Engineering, Beijing University of Technology, Beijing 100022,Key Laboratory of Advanced Functional Materials of China Education Ministry, Department of Materials Science and Engineering, Beijing University of Technology, Beijing 100022,Key Laboratory of Advanced Functional Materials of China Education Ministry, Department of Materials Science and Engineering, Beijing University of Technology, Beijing 100022 and Key Laboratory of Advanced Functional Materials of China Education Ministry, Department of Materials Science and Engineering, Beijing University of Technology, Beijing 100022
Abstract:
Keywords:hydrothermal method  K0  5Bi0  5TiO3  lead-free piezoelectric ceramic
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