| 纳米晶构筑一维多孔氧化锌的合成与表征 |
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| 引用本文： | 贾志刚,岳林海,郑遗凡,徐铸德.纳米晶构筑一维多孔氧化锌的合成与表征[J].无机化学学报,2007,23(7):1277-1281. |
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| 作者姓名： | 贾志刚 岳林海 郑遗凡 徐铸德 |
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| 作者单位： | 1. 浙江大学化学系,杭州,310027
2. 浙江工业大学化学工程与材料学院,杭州,310014 |
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| 摘 要： | One-dimensional porous zinc oxide was prepared via the calcination of zinc oxalate precursor obtained by solvothermal method. The products were characterized by XRD, SEM, TEM, photoluminescence (PL) spectrum and nitrogen adsorption-desorption. The results show that the obtained zinc oxide sample is porous and constructed by nanoparticles about 30 nm in size. The specific surface area and total pore volume are 126 m2·g-1 and 0.13 cm3·g-1, respectively． The PL properties related with defects in ZnO nanoparticles were discussed for porous zinc oxide samples.
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| 关 键 词： | 氧化锌 草酸锌 纳米晶 多孔材料 |
| 文章编号： | 1001-4861（2007）07-1277-05 |
| 修稿时间： | 2007-03-082007-05-09 |
Preparation and Characterization of One-dimensional Porous Zinc Oxide Constructed by Nanocrystal |
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| JIA Zhi-Gang,YUE Lin-Hai,ZHENG Yi-Fan and XU Zhu-De.Preparation and Characterization of One-dimensional Porous Zinc Oxide Constructed by Nanocrystal[J].Chinese Journal of Inorganic Chemistry,2007,23(7):1277-1281. |
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| Authors: | JIA Zhi-Gang YUE Lin-Hai ZHENG Yi-Fan and XU Zhu-De |
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| Institution: | Chemisty Department, Zhejiang University, Hangzhou 310027;College of Chemical Engineering and Materials, Zhejiang University of Technology, Hangzhou 310014 |
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| Abstract: | |
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| Keywords: | zinc oxide zinc oxalate nanocrystalline porous material |
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