| 高分散纳米二氧化钛混合晶体的合成、结构与光催化性能 |
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| 引用本文： | 王振兴,丁士文,张美红.高分散纳米二氧化钛混合晶体的合成、结构与光催化性能[J].无机化学学报,2005,21(3):437-440. |
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| 作者姓名： | 王振兴 丁士文 张美红 |
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| 作者单位： | 河北大学化学与环境科学学院,保定,071002 |
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| 基金项目： | 河北省自然科学基金重点资助项目(No.202104) |
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| 摘 要： | Using TiCl4 and urea as the raw materials and nanometric carbon black as plate, nanometric mix-crystals of rutile and anatase TiO2 were prepared at 100 ℃ for 10～180 min by homogeneous precipitation method. The effects of pH on the ratio of nanometer TiO2 mix-crystals were also discussed. TEM measurement indicates that the TiO2 is spherical particles, and the average diameter of the particles is 20 nm. XRD and TG-DTA were also used to characterize the nanometer mix-crystal materials. The photocatalytic experiment show that the mix-crystal material has the best photocatalytic reactivity. After being irradiated under the sunlight for 40 min, the compound can completely degrade the acid-red 3R.
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| 关 键 词： | 高分散纳米二氧化钛 混晶 制备 光催化性能 |
| 文章编号： | 1001-4861(2005)03-0437-04 |
| 收稿时间： | 2004/8/23 0:00:00 |
| 修稿时间： | 2004年8月23日 |
Synthesis, Structure and Photocatalysis of Nano-TiO2 Mixed Crystals |
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| WANG Zhen-Xing,DING Shi-Wen and ZHANG Mei-Hong.Synthesis, Structure and Photocatalysis of Nano-TiO2 Mixed Crystals[J].Chinese Journal of Inorganic Chemistry,2005,21(3):437-440. |
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| Authors: | WANG Zhen-Xing DING Shi-Wen and ZHANG Mei-Hong |
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| Institution: | College of Chemistry and Environmental Science, Hebei University, Baoding 071002,College of Chemistry and Environmental Science, Hebei University, Baoding 071002 and College of Chemistry and Environmental Science, Hebei University, Baoding 071002 |
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| Abstract: | |
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| Keywords: | nano-TiO2 mix-crystal preparation photocatalys |
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