| 硅化钴的简单固相合成与磁学性能 |
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| 引用本文： | 朱炳龙,陆铃鲸,戴伟城,张赐阳,方礼炜,王迪,王佳健.硅化钴的简单固相合成与磁学性能[J].无机化学学报,2019,35(5):876-880. |
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| 作者姓名： | 朱炳龙 陆铃鲸 戴伟城 张赐阳 方礼炜 王迪 王佳健 |
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| 作者单位： | 江苏理工学院化学与环境工程学院 |
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| 基金项目： | 中国国家社会发展基金（No.BE2016657）和江苏省高等学校自然科学基金（No.16KJA43007）资助 |
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| 摘 要： | 使用Co_3O_4、金属镁和硅为原料在不锈钢高压釜750℃反应得到立方相的硅化钴(CoSi)。所得样品的结构和形貌利用X射线粉末衍射(XRD)、透射电子显微镜(TEM)和场发射扫描电子显微镜(FESEM)等手段表征。XRD结果表明,所得样品为立方相CoSi,晶格常数为a=0.445 5 nm。此外,研究了CoSi样品的磁性和抗氧化性能,结果表明通过上述方法制备得到的硅化钴材料具有铁磁性,在600℃以下具有较好的稳定性和抗氧化性能。
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| 关 键 词： | 固相反应 陶瓷 X射线衍射 电子显微镜 纳米颗粒 |
| 收稿时间： | 2018/10/25 0:00:00 |
| 修稿时间： | 2019/3/28 0:00:00 |
Facile Solid-State Synthesis and Magnetic Properties of Cobalt Monosilicide |
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| ZHU Bing-Long,LU Ling-Jing,DAI Wei-Cheng,ZHANG Ci-Yang,FANG Li-Wei,WANG Di and WANG Jia-Jian.Facile Solid-State Synthesis and Magnetic Properties of Cobalt Monosilicide[J].Chinese Journal of Inorganic Chemistry,2019,35(5):876-880. |
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| Authors: | ZHU Bing-Long LU Ling-Jing DAI Wei-Cheng ZHANG Ci-Yang FANG Li-Wei WANG Di and WANG Jia-Jian |
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| Institution: | School of Chemistry and Environment Engineering, Jiangsu University of Technology, Changzhou, Jiangsu 213001, China,School of Chemistry and Environment Engineering, Jiangsu University of Technology, Changzhou, Jiangsu 213001, China,School of Chemistry and Environment Engineering, Jiangsu University of Technology, Changzhou, Jiangsu 213001, China,School of Chemistry and Environment Engineering, Jiangsu University of Technology, Changzhou, Jiangsu 213001, China,School of Chemistry and Environment Engineering, Jiangsu University of Technology, Changzhou, Jiangsu 213001, China,School of Chemistry and Environment Engineering, Jiangsu University of Technology, Changzhou, Jiangsu 213001, China and School of Chemistry and Environment Engineering, Jiangsu University of Technology, Changzhou, Jiangsu 213001, China |
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| Abstract: | |
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| Keywords: | solid-state reactions ceramics X-ray diffraction electron microscopy nanoparticles |
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