| 三维花状Fe_2(MoO_4)_3微米球的水热制备及电化学性能 |
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| 引用本文： | 郑浩,李琳,高虹,张晴,王石泉,冯传启.三维花状Fe_2(MoO_4)_3微米球的水热制备及电化学性能[J].无机化学学报,2014,30(12):2761-2766. |
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| 作者姓名： | 郑浩 李琳 高虹 张晴 王石泉 冯传启 |
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| 作者单位： | 安顺学院功能材料与资源化学重点实验室, 安顺 561000;有机化工新材料湖北省协同创新中心, 武汉 430062;安顺学院功能材料与资源化学重点实验室, 安顺 561000;有机化工新材料湖北省协同创新中心, 武汉 430062;有机化工新材料湖北省协同创新中心, 武汉 430062;湖北大学有机功能分子合成与应用教育部重点实验室, 武汉 430062;有机化工新材料湖北省协同创新中心, 武汉 430062;湖北大学有机功能分子合成与应用教育部重点实验室, 武汉 430062;有机化工新材料湖北省协同创新中心, 武汉 430062;湖北大学有机功能分子合成与应用教育部重点实验室, 武汉 430062;安顺学院功能材料与资源化学重点实验室, 安顺 561000;有机化工新材料湖北省协同创新中心, 武汉 430062;湖北大学有机功能分子合成与应用教育部重点实验室, 武汉 430062 |
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| 基金项目： | 贵州省科学技术厅、安顺市人民政府、安顺学院联合基金项目(NO.LKA [2013]17)资助项目. |
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| 摘 要： | 以Fe Cl3·7H2O和Na2Mo O4为原料,采用水热合成法制备三维花状Fe2(Mo O4)3微米球。探讨不同合成温度对样品形貌的影响,利用XRD、SEM和EDS等分析技术对样品的结构、形貌进行了表征,对该材料的电化学性能进行了测试。结果表明:Fe2(Mo O4)3微米球是由二维纳米片自组装而成的花状结构,合成温度为160℃时,制备的样品具有良好的电化学性能,当电流密度为100 m A·g-1,首次放电比容量为1 431 m Ah·g-1;并具有较好的循环性能和倍率性能。并对160℃合成样品表现较好电化学性能的原因进行了探讨。
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| 关 键 词： | Fe2(Mo O4)3 水热合成 锂离子电池 负极材料 |
| 收稿时间： | 2014/6/13 0:00:00 |
| 修稿时间： | 2014/7/22 0:00:00 |
3D Flower-Like Fe2(MoO4)3 Micron-Spheres: Synthesis and Applications in Lithium-Ion Batteries |
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| ZHENG Hao,LI Lin,GAO Hong,ZHANG Qing,WANG Shi-Quan and FENG Chuan-Qi.3D Flower-Like Fe2(MoO4)3 Micron-Spheres: Synthesis and Applications in Lithium-Ion Batteries[J].Chinese Journal of Inorganic Chemistry,2014,30(12):2761-2766. |
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| Authors: | ZHENG Hao LI Lin GAO Hong ZHANG Qing WANG Shi-Quan and FENG Chuan-Qi |
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| Institution: | Key Laboratory of Functional Materials and Chemistry for Performance and Resource of Guizhou Education Department, Anshun University, Anshun, Guizhou 561000, China;Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials, Hubei University, Wuhan 430062, China;Key Laboratory of Functional Materials and Chemistry for Performance and Resource of Guizhou Education Department, Anshun University, Anshun, Guizhou 561000, China;Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials, Hubei University, Wuhan 430062, China;Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials, Hubei University, Wuhan 430062, China;Key Laboratory for the Synthesis and Application of Organic Functional Molecules, Ministry of Education, Hubei University, Wuhan 430062, China;Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials, Hubei University, Wuhan 430062, China;Key Laboratory for the Synthesis and Application of Organic Functional Molecules, Ministry of Education, Hubei University, Wuhan 430062, China;Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials, Hubei University, Wuhan 430062, China;Key Laboratory for the Synthesis and Application of Organic Functional Molecules, Ministry of Education, Hubei University, Wuhan 430062, China;Key Laboratory of Functional Materials and Chemistry for Performance and Resource of Guizhou Education Department, Anshun University, Anshun, Guizhou 561000, China;Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials, Hubei University, Wuhan 430062, China;Key Laboratory for the Synthesis and Application of Organic Functional Molecules, Ministry of Education, Hubei University, Wuhan 430062, China |
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| Abstract: | |
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| Keywords: | Fe2(MoO4)3 hydrothermal synthesis lithium ion batteries anode material |
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