| 氢氧化锌合苯甲酸层状化合物的水热合成与表征 |
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| 引用本文： | 苗建英,王宏社,赵立芳,刘宗怀.氢氧化锌合苯甲酸层状化合物的水热合成与表征[J].无机化学学报,2006,22(5):900-904. |
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| 作者姓名： | 苗建英 王宏社 赵立芳 刘宗怀 |
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| 作者单位： | 1. 宝鸡文理学院化学化工系,宝鸡,721007
2. 陕西师范大学化学与材料科学学院,西安,710062 |
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| 基金项目： | 国家自然科学基金;陕西省教育厅资助项目 |
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| 摘 要： | The organic-inorganic layered compound zinc hydroxide-benzoic acid with basal spacing of 1.92 nm was synthesized hydrothermally using amorphous Zn(OH)2 and benzoic acid at the reaction temperature of 90～130 ℃, the molar ratio of C6H5COOH/Zn(Containing 6 mmol of Zn) of 0.4～0.6, 20 mL H2O and the reaction time of 6 h. The character, structure, particle morphology and chemical composition of the layered compound were characterized by means of XRD, TG-DTA, SEM, TEM and elemental analysis. The results indicate that the layered compound is of plate-like morphology and that with the temperature raising of hydrothermal synthesis, the particle of plate-like piece becomes smaller. The chemical formula of the layered compound could be written as Zn(OH)2-y·(C6H5COO)y·0.3H2O, 0.36≤y≤0.54.
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| 关 键 词： | 层状化合物 氢氧化锌合苯甲酸 水热合成 |
| 文章编号： | 1001-4861(2006)05-0900-05 |
| 收稿时间： | 2005-10-31 |
| 修稿时间： | 2005-12-30 |
Hydrothermal Synthesis and Characterization of the Layered Compound Zinc Hydroxide-Benzoic Acid |
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| MIAO Jian-Ying,WANG Hong-She,ZHAO Li-Fang and LIU Zong-Huai.Hydrothermal Synthesis and Characterization of the Layered Compound Zinc Hydroxide-Benzoic Acid[J].Chinese Journal of Inorganic Chemistry,2006,22(5):900-904. |
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| Authors: | MIAO Jian-Ying WANG Hong-She ZHAO Li-Fang and LIU Zong-Huai |
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| Abstract: | |
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| Keywords: | layered compound zinc hydroxide-benzoic acid hydrothermal synthesis |
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