| 无机微孔晶体AlPO_4-CJ_1合成与性能研究Ⅰ. |
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| 引用本文： | 于龙,庞文琴.无机微孔晶体AlPO_4-CJ_1合成与性能研究Ⅰ.[J].无机化学学报,1991(4). |
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| 作者姓名： | 于龙 庞文琴 |
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| 作者单位： | 吉林大学合成与催化研究所 长春130023
(于龙)，吉林大学合成与催化研究所 长春130023(庞文琴) |
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| 摘 要： | 自从八十年代美国UCC首次合成出非硅铝酸盐的AlPO_4-n系列分子筛以米,由于其特殊的骨架结构和物化性质,引起人们的广泛重视.我们用乙二胺基乙醇作模板剂合成出AlPO_4-CJ_1.经多晶X射线衍射,红外光谱及扫描电镜等结构表征,证明其为纯的,新型无机微孔晶体,吸附实验证明其具有4(?)的孔道.AlPO_4-CJ_1的制备:反应物摩尔配比:1.0Al_2O_3:1.0F_2O_5:(1.0-1.8)乙二胺基乙醇:(90-120)H_2O.以铝源硫酸铝水溶液(含Al_2O_37.04％)];磷源(磷酸铵);有机胺;水的次
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| 关 键 词： | 合成 孔 无机晶体 |
STUDY ON THE SYNTHESIS AND PROPERTIES OF INORGANIC MICROPOROUS CRYSTAL A1PO_4-CJ_1 |
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| Yu Long Pang Wenqin.STUDY ON THE SYNTHESIS AND PROPERTIES OF INORGANIC MICROPOROUS CRYSTAL A1PO_4-CJ_1[J].Chinese Journal of Inorganic Chemistry,1991(4). |
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| Authors: | Yu Long Pang Wenqin |
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| Institution: | Institute of Synthesis and Catalysis. Jilin University. Changchun 130023 |
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| Abstract: | In this paper, we have synthesized inorganic microporous crystal A1PQ4-CJ1 by hydrothermal crystallization from A12O3-P2O5-N, N-diethylanolamine-H2O system. We verified that it is new crystal and studied its infrared spectrum and got its shape by SEM. It is demonstrated that it has channel structure by measurement of DT-TG analysis and adsorption properties. |
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| Keywords: | synthesis pore inorganic crystal |
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