| 草酸锌空心纳米结构的一步固相合成及其表征 |
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| 引用本文： | 曹亚丽,刘浪,贾殿赠,忻新泉.草酸锌空心纳米结构的一步固相合成及其表征[J].中国化学,2005,23(5):539-542. |
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| 作者姓名： | 曹亚丽 刘浪 贾殿赠 忻新泉 |
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| 作者单位： | 新疆大学应用化学研究所，乌鲁木齐 830046;南京大学配位化学国家重点实验室，南京 210093 |
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| 摘 要： | 本文利用醋酸锌和草酸的一步低热固相化学反应制备了草酸锌空心纳米球，并通过在该反应体系中加入表面活性剂聚乙二醇400得到了草酸锌空心纳米链。采用X-射线粉末衍射（XRD）、透射电镜（TEM）、高倍透射电镜(HRTEM)、扫描电镜(SEM)、红外(IR) 以及热重-差热(TG/DTA)分析对所合成的样品进行了表征.
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| 关 键 词： | 空心结构 一步固相反应 草酸锌 纳米材料 |
| 收稿时间： | 2004-4-22 |
| 修稿时间： | 2005-1-28 |
One‐step Solid‐state Synthesis and Characterization of Two Kinds of ZnC2O4·2H2O Hollow Nanostructures |
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| Cao Ya‐Li,Liu Lang,Jia Dian‐Zeng,Xin Xin‐Quan.One‐step Solid‐state Synthesis and Characterization of Two Kinds of ZnC2O4·2H2O Hollow Nanostructures[J].Chinese Journal of Chemistry,2005,23(5):539-542. |
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| Authors: | Cao Ya‐Li Liu Lang Jia Dian‐Zeng Xin Xin‐Quan |
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| Abstract: | Two kinds of zinc oxalate dihydrate (ZnC2O4·2H2O) hollow nanostructures were synthesized successfully by a simple one‐step solid‐state reaction. ZnC2O4·2H2O hollow nanospheres were obtained via grinding zinc acetate and oxalic acid, while ZnC2O4·2H2O hollow nanochains were generated by the analogous reaction under the presence of a surfactant PEG 400. The as‐prepared samples were characterized by XRD, TEM, HRTEM, SEM, IR and TG/DTA |
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| Keywords: | hollow nanostructure one‐step solid state reaction zinc oxalate nanomaterial |
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