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Structure, thermal behavior, and IR investigation of a new organic sulfate
Authors:Taha Guerfel  Mohamed Bdiri  Amor Jouini
Institution:(1) Laboratoire de Chimie du Solide, Département de Chimie, Faculté des Sciences de Monastir, Université du Centre, 5000 Monastir, (Tunisie). E-mail
Abstract:1-(2-ammoniumethyl) piperazinium] sulfate denoted PIPS has a monoclinic unit cell. The parameters are: a = 6.6521(3), b = 7.8756(5), c = 19.197(1) Å, beta = 94.43(1)° and the space group is P21/n. The preparation, thermal analysis, and IR spectrometric investigation are described. The PIPS structure exhibits a complex three-dimensional network of H-bonds connecting all its components.
Keywords:organic sulfate  crystal structure  DTA/TG/DSC  vibrational spectra
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