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The graphite phase derived from polyimide at low temperature
Authors:Xianbiao Wang  Zhen Li
Institution:School of Materials Science and Chemical Engineering, Anhui University of Architecture, 856 Jin Zhai RD, Hefei, Anhui 230022, People’s Republic of China Advanced Building Materials Anhui Key Laboratory, Anhui University of Architecture, 856 Jin Zhai RD, Hefei, Anhui 230022, People’s Republic of China
Abstract:This paper reports a novel method to produce the graphite phase derived from polyimide using Ni(Ac)2 as catalyst at about 800 °C. The graphitization behavior was characterized by FTIR, X-ray diffraction, Raman spectra and N2 sorption measurements. The results showed that β-cyclodextrin promoted the catalytic effect of Ni(Ac)2 in graphitizing process, increased the degree of graphitization and micropore volume. The graphite structure was confirmed the pores distributed uniformly throughout by SEM.
Keywords:61  46  Hk  81  05  Uw  81  05  Kf  81  05  Rm
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