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三指标值法快速筛查不合格植物油
引用本文:何文绚,洪贵水,方润,蔡仙春,黄声.三指标值法快速筛查不合格植物油[J].光谱学与光谱分析,2015,35(4):1001-1009.
作者姓名:何文绚  洪贵水  方润  蔡仙春  黄声
作者单位:1. 闽江学院化学与化学工程系,福建 福州 350108
2. 福建省工商行政管理局, 福建 福州 350003
基金项目:福建省科技厅项目(2012Y0053);福州市科技局市科技局项目(2012-S-153);福建教育厅基金项目(JA12261);James and Susan He Foundation项目资助
摘    要:通过测定南方地区常用的花生油、玉米油、菜籽油、大豆油、葵花油、茶籽油、橄榄油等植物油以及地沟油和过期植物油的A3005(代表不饱和度)、A985(代表共轭脂肪酸含量)、A960+A985(代表反式脂肪酸含量)三个指标值,得到了合格植物油三个指标值设定范围。在此基础上,建立快速筛查不合格植物油(过期、添加低价油、添加地沟油)的方法,有效地提高了植物油的监控效率。利用该法筛查出的若干疑不合格油,通过脂肪酸构成法和11, 12, 13, 17脂肪酸含量判定法等,均证实它们是掺杂油或过期油,几种检测方法的结合应用,可进一步推断植物油不合格的原因。

关 键 词:植物油  筛查  红外光谱  ATR    
收稿时间:2014-01-06

Three-Iindex-Value Method for Rapid Screening Unqualified Vegetable Oil
HE Wen-xuan , HONG Gui-shui , FANG Run , CAI Xian-chun , HUANG Sheng.Three-Iindex-Value Method for Rapid Screening Unqualified Vegetable Oil[J].Spectroscopy and Spectral Analysis,2015,35(4):1001-1009.
Authors:HE Wen-xuan  HONG Gui-shui  FANG Run  CAI Xian-chun  HUANG Sheng
Institution:1. Department of Chemistry and Chemical Engineering, Minjiang University, Fuzhou 350108, China2. Fujian Provincial Administration for Industry and Commerce, Fuzhou 350003, China
Abstract:In the present study, by measuring the A3 005 (representing unsaturation), A985 (representing conjugated fatty acids), A960+A985 (representing trans-fatty acid ) of southern common vegetable oils (peanut oil, corn oil, canola oil, soybean oil, sunflower oil, tea seed oil and olive oil), “waste oil” and overdue vegetable oils, the pass-setting-range of these three index values for the vegetable oils was obtained. On this basis, a method for rapid screening unqualified vegetable oil (expired, adding low-cost oil, adding “waste oil”) was established. The method effectively improved the monitoring efficiency of vegetable oil. With this method of screening a number of suspected substandard oils were proved unqualified by determination of fatty acid composition and 11, 12, 13, 17 fatty acid content. Through the combination of several detection methods, the causes for disqualification of vegetable oils can be further inferred.
Keywords:Vegetable oil  Screen  IR  A T R
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