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[PMo9V3O40]6-硫代物的合成及光谱研究
引用本文:陈达贵,张汉辉,杨融生,孙瑞卿,杨齐瑜,余秀芬.[PMo9V3O40]6-硫代物的合成及光谱研究[J].光谱学与光谱分析,2000,20(5):712-714.
作者姓名:陈达贵  张汉辉  杨融生  孙瑞卿  杨齐瑜  余秀芬
作者单位:福州大学化学系,350002,福州
基金项目:国家重点实验室基金,990021,
摘    要:通过H2S与杂多化合物(NH4)4H2PM 9V3O40]·10H2O在DMF中反应合成了其硫代产物,并对其进行了红外和拉曼光谱表征.

关 键 词:杂多化合物  钒异金属硫桥簇合物  硫化物  光谱

ynthesis and Spectroscopic Studies of the Oxothio Heteropolyanion of [PMo9V3O40]6-
Dagui CHEN,Hanhui ZHANG,Rongsheng YANG,Ruiqing SUN,Qiyu YANG,Xiufen YU.ynthesis and Spectroscopic Studies of the Oxothio Heteropolyanion of [PMo9V3O40]6-[J].Spectroscopy and Spectral Analysis,2000,20(5):712-714.
Authors:Dagui CHEN  Hanhui ZHANG  Rongsheng YANG  Ruiqing SUN  Qiyu YANG  Xiufen YU
Institution:Department of Chemistry, Fuzhou University, 350002 Fuzhou.
Abstract:Some compounds were obtained through addition H2S to the heteropoly-compound (NH4)4H2PMo9V3O40].10H2O in dimethyformamide. The FTIR spectrum and NIR FT-Raman spectrum of these compounds were investigated. The spectroscopic studies of the compound II showed that it is a oxothio heteropoly-compound.
Keywords:Heteropolyanion    FTIR spectra    NIR FT-Raman s pectra
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