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原子吸收光谱法测定抗肿瘤中成药中微量元素
引用本文:刘彦明,王辉,韩金土,娄志鸽,乐世平.原子吸收光谱法测定抗肿瘤中成药中微量元素[J].光谱学与光谱分析,2006,26(9):1728-1731.
作者姓名:刘彦明  王辉  韩金土  娄志鸽  乐世平
作者单位:信阳师范学院化学化工学院,河南,信阳,464000
基金项目:河南省高校创新人才培养项目 , 河南省杰出青年科学基金 , 河南省自然科学基金
摘    要:利用原子吸收光谱法测定了复方天仙胶囊、消癌平片、参灵蓝胶囊、至灵胶囊和参莲胶囊5种抗肿瘤中成药中的15种微量元素.详细讨论了消化液(混酸)种类、混酸比例、消化时间及消化液体积对测定结果的影响.结果表明:5种抗癌中成药中,Ca,Mg,K,Na,Fe,Zn,Mn,Co和Ni的含量较为丰富.

关 键 词:原子吸收光谱法  抗肿瘤中成药  微量元素
文章编号:1000-0593(2006)09-1728-04
收稿时间:2005-05-09
修稿时间:2005-08-26

Determination of 15 Trace Elements in Antineoplastic Traditional Chinese Medicine by Atomic Absorption Spectrometry
LIU Yan-ming,WANG Hui,HAN Jin-tu,LOU Zhi-ge,YUE Shi-ping.Determination of 15 Trace Elements in Antineoplastic Traditional Chinese Medicine by Atomic Absorption Spectrometry[J].Spectroscopy and Spectral Analysis,2006,26(9):1728-1731.
Authors:LIU Yan-ming  WANG Hui  HAN Jin-tu  LOU Zhi-ge  YUE Shi-ping
Institution:College of Chemistry and Chemical Engineering, Xinyang Normal University, Xinyang 464000, China
Abstract:Five kinds of antineoplastic traditional Chinese medicines including fufangtianxian capsule, xiaoaiping tablet, zhiling capsule, shenlian capsule and shenlinglan capsule were digested with HNO3-HCl mixed acid. The fifteen trace elements including calcium, magnesium, potassium, sodium, iron, zinc, manganese, cobalt, nickel, chromium, silver, copper, strontium, cadmium and lead in the above-mentioned drugs were determined by atomic adsorption spectrometry. The effects of the kinds of mixed acid, the ratio of HNO3 to HCl in the mixed acid, the volume of digesting solution and the digesting time were also investigated in detail. The results obtained show that the concentrations of Ca, Mg, K, Na, Fe, Zn, Mn, Co and Ni in the five kinds of antineoplastic Chinese traditional medicines are higher than those of other elements.
Keywords:Atomic adsorption spectrometry  Antineoplastic Chinese traditional medicines  Trace elements
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