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痕量挥发性有机物的高场不对称波形离子迁移谱研究
作者姓名:Li Z  Lin BT  Kong DY  Chen CL  Cheng YP  Wang HQ  Mei T
作者单位:1. 中国科学院合肥智能机械研究所,传感技术国家重点实验室,安徽合肥,230031;中国科学技术大学自动化系,安徽合肥,230027
2. 中国科学院合肥智能机械研究所,传感技术国家重点实验室,安徽合肥,230031
基金项目:国家(863计划)项目(2007AA04Z341); 国家自然科学基金项目(60871037)资助
摘    要:高场不对称波形离子迁移谱(high-field asymmetric waveform ion mobility spectrometry,FAIMS)技术是一种快速、高灵敏的痕量物质检测技术.利用自制的高场不对称波形离子迁移谱仪分别对丙酮、苯和甲苯样品进行了检测,结果表明三种挥发性物质在谱图中的分离效果优于传统离子迁...

关 键 词:高场不对称波形离子迁移谱  痕量挥发性有机物

FAIMS of trace volatile organic compounds
Li Z,Lin BT,Kong DY,Chen CL,Cheng YP,Wang HQ,Mei T.FAIMS of trace volatile organic compounds[J].Spectroscopy and Spectral Analysis,2011,31(1):12-15.
Authors:Li Zhuang  Lin Bing-Tao  Kong De-Yi  Chen Chi-Lai  Cheng Yu-Peng  Wang Huan-Qin  Mei Tao
Institution:LI Zhuang1,2,LIN Bing-tao1,KONG De-yi1*,CHEN Chi-lai1,CHENG Yu-peng1,WANG Huan-qin1,MEI Tao1 1.Institute of Intelligent Machines,Chinese Academy of Sciences,State Key Laboratory of Transducer Technology,Hefei 230031,China 2.Department of Automation,University of Science and Technology of China,Hefei 230027,China
Abstract:FAIMS is a fast and high sensitive technique for detecting trace volatile organic compounds. Spectra of acetone, benzene and toluene were obtained on a homemade high-field asymmetric waveform ion mobility spectrometer and they can be easily separated in the spectra. Three xylene isomeric compounds were also successfully separated in FAIMS. Effect of carrier gas flow rate on the ion intensity was analyzed, and the optimal flow rate of carrier gas was 220 L x h(-1) which can be used for the optimization of FAIMS instrument. The detection limit for acetone is 100 ng x L(-1) that is an order of magnitude lower than the foreign traditional IMS.
Keywords:FAIMS  Trace volatile organic compounds(VOC)  
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