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微量脉冲进样-火焰原子吸收光谱法测定螺旋藻中的微量元素
引用本文:程存归,洪庆红,李丹婷,范勐海,蔡小丹.微量脉冲进样-火焰原子吸收光谱法测定螺旋藻中的微量元素[J].光谱学与光谱分析,2006,26(9):1735-1737.
作者姓名:程存归  洪庆红  李丹婷  范勐海  蔡小丹
作者单位:1. 浙江师范大学化学与生命科学学院,浙江,金华,321004
2. 浙江师范大学化学与生命科学学院,浙江,金华,321004;金华大学材料与化工学院,浙江,金华,321017
摘    要:将微量脉冲进样技术和火焰原子吸收光谱法结合,对钝顶螺旋藻中的Ni,Zn,Mn,Cu,Mg,Fe,Ca和Pb等微量元素进行了测定.结果显示钝顶螺旋藻含有丰富的镁,锌,铁及钙,铜.该方法的加标回收率为96.58%~106.12%,RSD<4.26%,具有良好的准确度和精密度.测定结果可为探讨钝顶螺旋藻中微量元素含量与其药效的相关性提供科学数据.

关 键 词:微量脉冲进样  火焰原子吸收光谱法  钝顶螺旋藻  微量元素
文章编号:1000-0593(2006)09-1735-03
收稿时间:2004-09-08
修稿时间:2005-01-18

Determination of Trace Elements in Spirulina Platensis (Notdst.) Geitl.by Flame Atomic Absorption Spectrometry Combined with Microsampling Pulse Nebulization Technique
CHENG Cun-gui,HONG Qing-hong,LI Dan-ting,FAN Meng-hai,CAI Xiao-dan.Determination of Trace Elements in Spirulina Platensis (Notdst.) Geitl.by Flame Atomic Absorption Spectrometry Combined with Microsampling Pulse Nebulization Technique[J].Spectroscopy and Spectral Analysis,2006,26(9):1735-1737.
Authors:CHENG Cun-gui  HONG Qing-hong  LI Dan-ting  FAN Meng-hai  CAI Xiao-dan
Institution:1. College of Chemistry and Life Science, Zhejiang Normal University, Jinhua 321004, China;2. College of Materials and Chemical Engineering, Jinhua University, Jinhua 321017, China
Abstract:The contents of trace elements Ni, Zn, Mn, Cu, Mg, Fe, Ca and Pb in Spirulina platensis (Notdst.) Geitl. were determined by flame atomic absorption spectrometry combined with microsampling pulse nebulization technique. The results of the determination show that Spirulina platensis (Notdst.) Geitl. are rich in the inorganic elements such as Mg, Zn, Fe, Ca and Cu. Its recovery ratio obtained by standard addition method ranged between 96.58% and 106.12%, and its RSD was lower than 4.26%. The result will provide scientific data for the study on the trace elements in Spirulina platensis (Notdst.) Geitl. and on their relativity of efficacy of medicine.
Keywords:Microsampling pulse nebulization  Flame atomic absorption spectrometry  Spirulina platensis (Notdst  ) Geitl    Trace elements
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