| 水杨酸镍配合物的合成和红外光谱研究 |
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| 引用本文： | 李良超,袁良杰,杨毅涌,张克立,孙聚堂.水杨酸镍配合物的合成和红外光谱研究[J].光谱学与光谱分析,2000,20(5):671-672. |
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| 作者姓名： | 李良超 袁良杰 杨毅涌 张克立 孙聚堂 |
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| 作者单位： | 武汉大学化学系,430072,武汉 |
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| 基金项目： | 国家自然科学基金资助课题!(No 2 9971 0 2 4 ) |
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| 摘 要： | 用流变相反应法合成了３个水杨酸镍配合物。通过元素分析、ＴＧ确定了这些配合物的组成，并对４０００～４００ｃｍ＾－１的主要红外光谱吸收峰进行了归属；红外光谱表明－水杨酸镍的羟基吸收峰明显地向高波数方向移动，证明其中有氢氧根存在。
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| 关 键 词： | 流变相 合成 红光光谱 水杨酸镍配合物 结构 |
Studies on Synthesis and IR Spectrum of Nickel Salicylates Complexes |
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| Liangchao LI,Liangjie YUAN,Yiyong YANG,Keli ZHANG,Jutang SUN.Studies on Synthesis and IR Spectrum of Nickel Salicylates Complexes[J].Spectroscopy and Spectral Analysis,2000,20(5):671-672. |
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| Authors: | Liangchao LI Liangjie YUAN Yiyong YANG Keli ZHANG Jutang SUN |
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| Institution: | Depart. of Chem., Wuhan University, 430072 Wuhan. |
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| Abstract: | Nickel salicylates complexes were synthesized with the rheologic phase reaction method. The composition of these complexes were confirmed by elemental analysis, TG and IR, the principal infrared absorption peaks were assigned for the region 4,000-400 cm-1. The IR spectra indicated that a hydroxyl group on Ni atom was occurred and so absorption peaks of hydroxyl group were shifted obviously to higher frequency in nickel monosalicylates. |
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| Keywords: | Nickel salicylates Rheologic phase Synthesis Infrared spectrum |
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