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A solid state pulsed NMR spectrometer
Authors:R K Shenoy  J Ramakrishna  K R Jeffrey
Institution:1. Department of Physics, Indian Institute of Science Bangalore, 560 012, India
3. Department of Physics, University of Guelph, Guelph, Ontario, Canada
Abstract:A 10 MHz pulsed NMR spectrometer, built using mostly solid state devices, is described. The pulse programmer provides 2-pulse, 3-pulse, saturation burst and Carr-Purcell sequences both in repetitive and manual modes of operation. The transmitter has a maximum power output of ~ 2 kW with a 75 Ω output impedance termination. The total gain of the receiver system is around 120 dB with a minimum band width of 2 MHz. The recovery time of the receiver is ~ 7 µsec. A two-channel boxcar integrator capable of working in the single channel, differential and double boxcar modes provides signal to noise ratio improvement. The sensitivity and the linearity of the boxcar integrator are ~ 2 mV and ~ 0.1% respectively.
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