Microstructural and electromagnetic properties of MnO2 coated nickel particles with submicron size |
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Authors: | Tang Bao-Lin He Jun Ji Tian-Hao and Wang Xin-Lin |
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Institution: | College of Chemical and Environmental Engineering,
Beijing Technology and Business University, Beijing 100048,
China; Division of Functional Material Research,
Central Iron
{$ &$ Steel Research Institute, Beijing 100081, China |
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Abstract: | Nickel particles with submicron size are prepared by using the
solvothermal method. These spheres are then coated with a layer of
MnO2 using the soft chemical method. The microstructure is
characterized by x-ray diffraction, transmission electron
microscopy, and scanning electron microscopy. Energy x-ray
dispersive spectrometry and high-resolution images show that the
granular composites have a classical core/shell structure with an
MnO2 superficial layer, no more than 10~nm in thickness. The
hysteresis measurements indicate that these submicron-size Ni
composite powders have small remanence and moderate coercivity. The
electromagnetic properties of the powders measured by a vector
network analyzer in a frequency range of 2--18~GHz are also reported
in detail. |
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Keywords: | core/shell microstructure submicron electromagnetic properties |
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