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Constant-load delayed fracture test of atmospherically corroded high strength steels
Authors:Eiji Akiyama  Katsuhiro Matsukado  Songjie Li  Kaneaki Tsuzaki
Institution:a National Institute for Materials Science, 1-2-1 Sengen, Tsukuba, Ibaraki, 305-0047, Japan
b Kobe Steel, Ltd., 15 Kinugaoka, Moka, Tochigi 321-4367, Japan
c University of Science and Technology Beijing, No. 30 Xueyuan Road, Haidian Zone, Beijing 100083, China
Abstract:Constant load tests of circumferentially notched round bar specimens of high strength steels after cyclic corrosion test and outdoor exposure have been performed to demonstrate that delayed fracture occurs when the hydrogen content from the environment, HE, exceeds the critical hydrogen content for delayed fracture, HC. During the constant load tests the humidity around the specimen was increased in stepwise manner to increase hydrogen entry. After fracture the specimen was kept at the humidity long enough to homogenize hydrogen in the specimen and to obtain more quantitative hydrogen content by thermal desorption analysis. HE of the fractured specimens was higher than HC, and HE of the specimens not fractured was lower than HC. This result confirms that the balance between HC and HE determines the occurrence of delayed fracture and that hydrogen-content-based evaluation of susceptibility to delayed fracture is reasonable. To certify the increase of HE with increase in humidity, electrochemical hydrogen permeation test was carried out. The hydrogen permeation current density was increased especially at 98%RH. Enhancement of hydrogen entry with increase in CCT number was also shown by the test.
Keywords:Hydrogen embrittlement  Delayed fracture  Atmospheric corrosion  High strength steel
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