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ICP-OES测定两种松树中的矿质元素
引用本文:赵宁,郭盘江,雷然,李云仙,陈玉惠.ICP-OES测定两种松树中的矿质元素[J].光谱实验室,2009,26(1):74-77.
作者姓名:赵宁  郭盘江  雷然  李云仙  陈玉惠
作者单位:云南省西南林学院基础部化学教研室,昆明市盘龙区白龙寺300号,650224
摘    要:采用HNO3-HF-HClO4湿法消解木材样品,电感耦合等离子体发射光谱法(ICP-OES)测定思茅松、云南松茎干中的Ca、Fe、K、Mg、P、Mn、Zn等矿质元素。结果表明,思茅松、云南松中的矿质元素表现为不同的含量顺序,思茅松中矿质元素含量为Ca〉K〉Zn〉Mg〉P〉Fe〉Mn,而云南松中矿质元素含量为Ca〉Fe〉K〉Mg〉P〉Mn〉Zn。该方法具有良好的准确度及精密度,加标回收率在95.63%—108%范围内,相对标准偏差(RSD)在0.3%—2.4%范围内,结果可靠,操作方便,可用于其他树木样品中相同矿质元素的测定。

关 键 词:电感耦合等离子体发射光谱法  思茅松  云南松  矿质元素

Determination of Mineral Elements in Two Pine Trees by ICP-OES
ZHAO Ning,Guo Pan-Jiang,LEI Ran,LI Yun-Xian,CHEN Yu-Hui.Determination of Mineral Elements in Two Pine Trees by ICP-OES[J].Chinese Journal of Spectroscopy Laboratory,2009,26(1):74-77.
Authors:ZHAO Ning  Guo Pan-Jiang  LEI Ran  LI Yun-Xian  CHEN Yu-Hui
Institution:Southwest Forest College;Kunming 650224;P.R.China
Abstract:HNO3-HF-HCIO4 was employed to digest the wood samples,the mineral elements Ca,Fe,K,Mg,P,Mn,and Zn in the stems of Pinus kesiya var.langbianensis and Pinus yunnanensis were analyzed by ICP-OES. The mineral elements in the Pinus kesiya var.langbianensis are in the order of Ca>K>Zn>Mg>P>Fe>Mn ,and in Pinus yunnanensis of Ca>Fe>K>Mg>P>Mn>Zn. This method is of accuracy with labeling recovery between 95.63% to 108% and with RSD between 0.3% to 2.4%. this method is easy to used for a reliable result,and can be ext...
Keywords:ICP-OES  Pinus Kesiya Var  Langbianensis  Pinus Yunnanensis  Mineral Elements    
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