|
|||||
|
|
| SPE-HPLC同时测定馒头中的4种直链烷基苯磺酸钠 | |
| 引用本文： | 贾松涛,周围,王波,解迎双,牛宏亮.SPE-HPLC同时测定馒头中的4种直链烷基苯磺酸钠[J].光谱实验室,2011,28(5):2411-2415. |
| 作者姓名： | 贾松涛 周围 王波 解迎双 牛宏亮 |
| 作者单位： | 1. 甘肃农业大学食品科学与工程学院 兰州市安宁区营门村1号730070 2. 甘肃农业大学食品科学与工程学院 兰州市安宁区营门村1号730070;甘肃出入境检验检疫局中心实验室 兰州市城关区嘉峪关东路387号730020 3. 甘肃出入境检验检疫局中心实验室 兰州市城关区嘉峪关东路387号730020 4. 西北师范大学地理与环境科学学院 兰州市730070 |
| 摘 要： | 建立了馒头中4种直链烷基苯磺酸钠高效液相色谱的测定方法。样品经甲醇和水提取后经过MAX复合阴离子交换小柱净化后,利用高效液相色谱进行检测。方法检出限为5μg/mL,4种直链烷基苯磺酸钠的检测波长为225nm,回收率为84.92%—99.28%,相对标准偏差为4.37%—5.93%。可以满足馒头中直链烷基苯磺酸钠检测的方法要求。 |
| 关 键 词： | 高效液相色谱法 固相萃取 直链烷基苯磺酸钠 馒头 |
Simultaneous Determination of 4 Kinds of Linear Alkylbenzene Sulfonates in Bun by SPE-HPLC |
|
| JIA Song-Tao,ZHOU Wei,WANG Bo,XIE Ying-Shuang,NIU Hong-Liang.Simultaneous Determination of 4 Kinds of Linear Alkylbenzene Sulfonates in Bun by SPE-HPLC[J].Chinese Journal of Spectroscopy Laboratory,2011,28(5):2411-2415. | |
| Authors: | JIA Song-Tao ZHOU Wei WANG Bo XIE Ying-Shuang NIU Hong-Liang |
| Institution: | JIA Song-Taoa ZHOU Weia,b WANG Bob XIE Ying-Shuangc NIU Hong-Liangaa(College of Food Science and Engineering,Gansu Agricultural University,Lanzhou 730070,P.R.China)b(Central Laboratory,Entry-Exit Inspection and Quarantine Bureau of Gansu,Lanzhou 730020,P.R.China)c(College of Geography and Environmental Science,Northwest Normal University,P.R.China) |
| Abstract: | A method for the determination of four kinds of linear alkylbenzene sulfonates in bun was established by high performance liquid chromatography（HPLC）.Samples were extracted by methanol and water,then purified by the complex anion exchange column of MAX,and were detected by HPLC.The detection limitations were 5μg/mL.Detection wavelength was 225nm.The recoveries ranged from 84.92% to 99.28%,with relative standard deviations between 4.37% and 5.93%.The results meets the need for the determination of four kinds of linear alkylbenzene sulfonates in bun. |
| Keywords: | HPLC Solid-Phase Extraction Linear Alkylbenzene Sulfonates Bun |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |