| 中成药中马兜铃酸A的UPLC/MS研究 |
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| 引用本文： | 周围,牛宏亮,王波,刘红卫,贾松涛,解迎双.中成药中马兜铃酸A的UPLC/MS研究[J].光谱实验室,2011,28(1):183-187. |
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| 作者姓名： | 周围 牛宏亮 王波 刘红卫 贾松涛 解迎双 |
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| 作者单位： | 甘肃出入境检验检疫局;甘肃农业大学食品科学与工程学院;甘肃省轻工业研究院;西北师范大学地理与环境科学学院; |
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| 摘 要： | 建立了中成药中马兜铃酸A的超高压液相色谱/质谱检测方法。测定结果表明,马兜铃酸A在超高压液相色谱/质谱的选择离子记录（SIR）中有较强的分子离子峰,检出限为0.1mg/kg,可以满足对中成药中马兜铃酸A测定要求。
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| 关 键 词： | 超高压液相色谱/质谱联用仪 中成药 马兜铃酸A |
Research of Aristolochic Acid A in Chinese Traditional Patent Medicine by UPLC/MS |
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| ZHOU Wei,NIU Hong-Liang,WANG Bo,LIU Hong-Wei,JIA Song-Tao,XIE Ying-Shuang.Research of Aristolochic Acid A in Chinese Traditional Patent Medicine by UPLC/MS[J].Chinese Journal of Spectroscopy Laboratory,2011,28(1):183-187. |
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| Authors: | ZHOU Wei NIU Hong-Liang WANG Bo LIU Hong-Wei JIA Song-Tao XIE Ying-Shuang |
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| Institution: | ZHOU Wei a,c NIU Hong-Liang b WANG Bo a LIU Hong-Wei a JIA Song-Tao c XIE Ying-Shuang da(Gansu Entry-Exit Inspection and Quarantine Bureau,Lanzhou 730020,P.R.China)b(Gansu Research Institute of Light Industry,Lanzhou 730000,P.R.China)c(Department of Food Science and Engineering,Gansu Agricultural University,Lanzhou 730070,P.R.China)d(Geographic and Environmental Science Institute,Northwest Normal University,P.R.China) |
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| Abstract: | The method of UPLC/MS for analysis of Aristolochic Acid A in Chinese traditional patent medicine was established.The Aristolochic Acid A in selected ion recording(SIR) of UPLC/MS had a strong molecular ion peak,and the detection limit was 0.1mg/kg.The sensitivity is high enough to determine Aristolochic Acid A in Chinese traditional patent medicine. |
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| Keywords: | UPLC/MS Chinese Traditional Patent Medicine Aristolochic Acid A |
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