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| MSA-DUO-ICP-AES测定菜园土壤中高关注重金属预处理探讨 | |
| 引用本文： | 唐志锟,钟志光,郭汉城,田琼,曹晓燕.MSA-DUO-ICP-AES测定菜园土壤中高关注重金属预处理探讨[J].光谱实验室,2010,27(2):749-753. |
| 作者姓名： | 唐志锟 钟志光 郭汉城 田琼 曹晓燕 |
| 作者单位： | 1. 广东出入境检验检疫局,广州市天河区珠江新城花城大道66号,510623 2. 清远出入境检验检疫局,广东省清远市,511515 3. 湛江出入境检验检疫局,广东省湛江市,524022 4. 佛山出入境检验检疫局,广东省佛山市,528000 |
| 基金项目： | 广东出入境检验检疫局科研项目资助(2009GDK49) |
| 摘 要： | 比较加入几种不同的混酸,用微波消解仪对土壤样品进行消解,采用双向视电感耦合发射光谱仪(DUO-ICP-AES)标准加入法(MSA)测定土壤中6项重金属元素含量。研究表明,HNO3-HClO4-HF-HCl处理土壤的效果比王水、HNO3-HF更佳,同时该法快速简单,回收率和精密度较好,干扰少,为土壤重金属含量的快速测定开辟了新方法。 |
| 关 键 词： | 土壤 重金属 微波消解 标准加入法 |
Study on Determination of Deep-Concerned Heavy Metal in Soil of Vegetable Lands by MSA-DUO-ICP-AES |
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| Tang Zhi-Kun,Zhong Zhi-Guang,Guo Han-Cheng,Tian Qiong,Cao Xiao-Yan.Study on Determination of Deep-Concerned Heavy Metal in Soil of Vegetable Lands by MSA-DUO-ICP-AES[J].Chinese Journal of Spectroscopy Laboratory,2010,27(2):749-753. | |
| Authors: | Tang Zhi-Kun Zhong Zhi-Guang Guo Han-Cheng Tian Qiong Cao Xiao-Yan |
| Institution: | Guangdong Entry-Exit Inspection & Quarantine Bureau;Guangzhou 510623;P.R.China;Qingyuan Entry-Exit Inspection & Quarantine Bureau;Qingyuan;Guangdong 511515;P.R.China;Zhanjiang Entry-Exit Inspection & Quarantine Bureau;Zhanjiang;Guangdong 524022;P.R.China;Foshan Entry-Exit Inspection & Quarantine Bureau;Foshan;Guangdong 528000;P.R.China |
| Abstract: | The soil was digested with different mixable acid.Six kinds of heavy metals in soil were determined by dual observation-inductively coupled plasma-atomic emission spectrometry associated with standard addition method.The results showed that using HNO3-HClO4-HF-HCl to digest soil samples was better.The new method is rapid,simple and with satisfactory precision and recovery. |
| Keywords: | Soil Heavy Metal Microwave Digestion Standard Addition Method |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |