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| 微波消解ICP-AES测定桔梗中微量元素 | |
| 引用本文： | 席晓岚,徐红,季宇飞,曾广铭,李明炬.微波消解ICP-AES测定桔梗中微量元素[J].光谱实验室,2010,27(3):884-887. |
| 作者姓名： | 席晓岚 徐红 季宇飞 曾广铭 李明炬 |
| 作者单位： | 1. 贵阳医学院化学教研室,贵阳市北京路9号,550004 2. 贵阳市环境监测中心站,贵阳市青云路304号,550002 3. 贵州神奇制药有限公司,贵阳市贵开路1号,550003 |
| 摘 要： | 采用微波消解样品,电感耦合等离子体-原子发射光谱法(ICP-AES)测定了中药材桔梗中Cu、Li、Mn、Co、Zn、Cr、Mg、Ga、Sr、Fe等微量元素的含量。在最佳仪器工作条件下,各元素的加标回收率在86.5%—111.0%,相对标准偏差RSD4.0%,实验结果可为桔梗中微量元素与其药效的相关性提供科学依据。 |
| 关 键 词： | 微波消解 电感耦合等离子体-原子发射光谱法 桔梗 微量元素 |
Determination of Trace Elements in Campanulaceae by ICP-AES with Microwave Digestion |
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| XI Xiao-Lan,XU Hong,JI Yu-Fei,ZENG Guang-Ming,LI Ming-Ju.Determination of Trace Elements in Campanulaceae by ICP-AES with Microwave Digestion[J].Chinese Journal of Spectroscopy Laboratory,2010,27(3):884-887. | |
| Authors: | XI Xiao-Lan XU Hong JI Yu-Fei ZENG Guang-Ming LI Ming-Ju |
| Institution: | b(Department of Chemistry,Guiyang Medical College,Guiyang 550004,P.R.China)a(Guiyang Environmental Monitoring Center Station,Guiyang 550002,P.R.China)b(Guizhou Shenqi Pharmaceutical Company Ltd.,Guiyang 550003,P.R.China) |
| Abstract: | The trace elements of Co,Cu,Ga,Cr,Li,Mn,Zn,Mg,Sr and Fe in the Chinese herbal medicine campanulaceae were determined by inductively coupled plasma atomic emission spectrometry（ICP-AES） with microwave digestion.Under the best working condition of the equipment,the elements recovery of standard addition is 86.5%—111.0% and the relative standard deviation （RSD） is less than 4.0%.The experimental results provide a scientific basis for the campanulaceae effect of trace elements and their relevance. |
| Keywords: | Microwave Digestion ICP-AES Campanulaceae Trace Elements |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |