| 苯甲酰脲类杀虫剂杀虫隆的合成及表征 |
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| 引用本文： | 冯晓亮,高鸿杰,谢建伟,谢泉.苯甲酰脲类杀虫剂杀虫隆的合成及表征[J].光谱实验室,2013(6):2984-2987. |
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| 作者姓名： | 冯晓亮 高鸿杰 谢建伟 谢泉 |
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| 作者单位： | 衢州学院化学与材料工程学院,浙江省衢州市九华路78号324000 |
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| 基金项目： | 浙江省公益性技术应用研究计划项目（NO.2011C31036） |
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| 摘 要： | 以对三氟甲氧基苯胺和二（三氯甲基）碳酸酯合成对三氟甲氧基苯基异氰酸酯,再与邻氯苯甲酰胺反应合成杀虫隆,二步反应收率合计84.7％,确定了用高效液相色谱测定产品含量的方法,产品纯度在99％以上.用IR、1HNMR及元素分析进行结构确证.
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| 关 键 词： | 杀虫隆 合成 表征 |
Synthesis and Characterization of Triflumuro,One Kind of Benzoylureas |
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| FENG Xiao-Liang,GAO Hong-Jie,XIE Jian-Wei,XIE Quan.Synthesis and Characterization of Triflumuro,One Kind of Benzoylureas[J].Chinese Journal of Spectroscopy Laboratory,2013(6):2984-2987. |
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| Authors: | FENG Xiao-Liang GAO Hong-Jie XIE Jian-Wei XIE Quan |
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| Institution: | (School of Chemical and Materkd Engineering, Quzhou University, Quzhou, Zhejiang 324000, P. R. China) |
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| Abstract: | 4-Trifluiormethoxy phenyl isocyanate （2） was synthesized by 4-（trifluorome-thoxy） aniline and triphosgene. Then,triflumuro（1）was synthesized by 2 and 2-chlorobenzamide. The overall yield was 84. 7%. Analysis of 1 was determined by HPLC and the purity of 1 is up to 99%. The structure of the product was identified by IR,^1HNMR and elemental analysis. |
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| Keywords: | Triflumuro Synthesis Characterization |
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