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拐枣七中原阿片碱的分离
引用本文:索建兰,张旭东.拐枣七中原阿片碱的分离[J].光谱实验室,2013(6):3260-3263.
作者姓名:索建兰  张旭东
作者单位:宝鸡文理学院化学化工系,陕西省宝鸡市高新大道一号720013
基金项目:陕西省科技发展计划项目(2012JM2019);陕西省重点实验室重点项目(2012JS008)
摘    要:用酸碱法从拐枣七中提取总生物碱,并测定其中原阿片碱的含量.从拐枣七中提取出总生物碱,用有机溶剂萃取法提取其中的原阿片碱,然后进行鉴定,鉴定包括熔点测定,呈色反应等.拐枣七中总生物碱含有隐品碱,别隐品碱,原阿片碱等多种碱,其中原阿片碱含量居多.

关 键 词:拐枣七  总生物碱  原阿片碱  有机溶剂萃取  呈色反应

Extraction of Total Alkaloids in Calligonum seven
Institution:SUO Jian-Lan ,XU Qing-Jie(Department of Chem.&. Chem. Eng. , Baoji University of Arts & Sciences, Baoji 721007, P. R. China)
Abstract:Extracting the total alkaloids from calligonum seven by acid-base method, and determining the content of protopine in the total alkaloids. The total alkaloids were extracted from calligonum seven by acid-base method, and the protopine was got by organic solvent extraction method. Melting point determination and color reaction were employed to appraisal it. Total alkaloids in calligonum seven contain cryptopine,allocryptopine, protopine and so on. And protopine is the main component in the total alkaloids.
Keywords:Calligonun Seven  Total Alkaloids  Protopine  Organic Solvent Extraction  ColorReaction
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